| 高效液相色谱法测定乌金胶囊中毛蕊异黄酮的含量 |
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| 引用本文： | 王慧,李洋,吕昉,凌水花,黄玉凤,张国庆. 高效液相色谱法测定乌金胶囊中毛蕊异黄酮的含量[J]. 药学实践杂志, 2015, 33(1): 53-54,57 |
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| 作者姓名： | 王慧 李洋 吕昉 凌水花 黄玉凤 张国庆 |
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| 作者单位： | 第二军医大学东方肝胆外科医院药材科, 上海 200438,第二军医大学东方肝胆外科医院药材科, 上海 200438,第二军医大学东方肝胆外科医院药材科, 上海 200438,第二军医大学东方肝胆外科医院药材科, 上海 200438,第二军医大学东方肝胆外科医院药材科, 上海 200438,第二军医大学东方肝胆外科医院药材科, 上海 200438 |
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| 摘 要： | 目的建立高效液相色谱法测定乌金胶囊中毛蕊异黄酮含量。方法色谱柱为ZORBA Bonus-RP(4.6mm×260mm,5μm)分析柱,流动相乙腈-水(含0.1%甲酸)梯度洗脱,柱温25℃,检测波长为260nm,流速1.0 ml/min,进样量10μl。结果毛蕊异黄酮在7.4~117.6μg/ml(r=1.000)浓度范围内呈良好线性关系,其回归方程为Y=34.002 X-3.451 2,回收率为95.24%(RSD=2.10%)。6批乌金胶囊中异黄酮含量在9.26~23.14μg/g之间。结论该方法简便、快速、准确,可用于乌金胶囊的质量控制。
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| 关 键 词： | 高效液相色谱法 毛蕊异黄酮 含量测定 乌金胶囊 |
| 收稿时间： | 2014-01-27 |
| 修稿时间： | 2014-04-11 |
Determination of calycosin contents in Wujin capsule by HPLC |
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| WANG Hui,LI Yang,L,#; Fang,LING Shuihu,HUANG Yufeng and ZHANG Guoqing. Determination of calycosin contents in Wujin capsule by HPLC[J]. The Journal of Pharmaceutical Practice, 2015, 33(1): 53-54,57 |
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| Authors: | WANG Hui,LI Yang,L&# Fang,LING Shuihu,HUANG Yufeng ZHANG Guoqing |
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| Affiliation: | Department of Pharmacy, Eastern Hepatobilliary Hospital, Second Military Medical University, Shanghai 200438, China,Department of Pharmacy, Eastern Hepatobilliary Hospital, Second Military Medical University, Shanghai 200438, China,Department of Pharmacy, Eastern Hepatobilliary Hospital, Second Military Medical University, Shanghai 200438, China,Department of Pharmacy, Eastern Hepatobilliary Hospital, Second Military Medical University, Shanghai 200438, China,Department of Pharmacy, Eastern Hepatobilliary Hospital, Second Military Medical University, Shanghai 200438, China and Department of Pharmacy, Eastern Hepatobilliary Hospital, Second Military Medical University, Shanghai 200438, China |
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| Abstract: | |
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| Keywords: | HPLC calycosin determination Wujin capsule |
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