| 远志中β-咔啉系生物碱的HPLC测定 |
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| 引用本文： | 金宝渊,朴政一.远志中β-咔啉系生物碱的HPLC测定[J].延边医学院学报,1993,16(1):63-65. |
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| 作者姓名： | 金宝渊 朴政一 |
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| 作者单位： | 延边医学院分析化学教研室，延边医学院分析化学教研室，延边医学院分析化学教研室，韩国汉城大学药学院，韩国汉城大学药学院 |
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| 摘 要： | 利用HPLC定量测定远志样品中的β-咔啉系生物碱:降哈尔满、哈尔满、perlolyrine、1-甲氧羰基—咔啉、1-乙氧羰基—咔啉、N_9-甲酰基哈尔满及1-丁氧羰基-咔啉。
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| 关 键 词： | 远志 咔啉类生物碱类 |
HPLC Determination of beta-Carboline Alkaloids in Polygala tenuifolia |
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| Jin Baoyuan.HPLC Determination of beta-Carboline Alkaloids in Polygala tenuifolia[J].Journal of Medical Science Yanbian University,1993,16(1):63-65. |
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| Authors: | Jin Baoyuan |
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| Abstract: | A HPLC method was developed for the determination of the β-carboline alkaloids in the rhizoma of polygala tenuifolia willdenow. Norharman, harman, perlolyrine, 1-carbomethoxyβ-carboline, 1-carboetoxy-β-carboline, N-formylharman, 1-caebobutoxy-β-carboline in the sample was determinated quantitatively by the method. A reverse phase system with Hiber Rp-18 (7m) column was employed with 0.05mol potassium phosphate buffer (pH=3.5): acetonitrile with gradient elution. The alkaloids were detected at 254nm. |
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| Keywords: | polygala tenuifolia carbolines alkaloids |
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