| 浓缩型咽炎颗粒(无糖型)质量标准研究 |
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| 引用本文： | 张沂,凌云,蔡清宇,杜栋逾. 浓缩型咽炎颗粒(无糖型)质量标准研究[J]. 中国药房, 2009, 0(6): 438-440 |
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| 作者姓名： | 张沂 凌云 蔡清宇 杜栋逾 |
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| 作者单位： | 海军总医院药剂科,北京市100037 |
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| 摘 要： | 目的:建立浓缩型咽炎颗粒(无糖型)的质量标准。方法:采用薄层色谱(TLC)法对方中玄参、北豆根、甘草进行定性鉴别;采用高效液相色谱法测定本制剂的有效成分蒙花苷的含量。结果:TLC斑点清晰、分离度高。蒙花苷进样量在4.64～69.6μg范围内与峰面积积分值呈良好线性关系(r=0.9999);平均加样回收率为98.65%,RSD=0.79%(n=6)。结论:所建标准可用于浓缩型咽炎颗粒(无糖型)的质量控制。
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| 关 键 词： | 浓缩型咽炎颗粒(无糖型) 薄层色谱法 高效液相色谱法 质量标准 |
Quality Standard of Yanyan Granules of Concentrated Sugar- free Type |
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| ZHANG Yi,LING Yun,CAI Qing-yu,DU Dong-yu. Quality Standard of Yanyan Granules of Concentrated Sugar- free Type[J]. China Pharmacy, 2009, 0(6): 438-440 |
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| Authors: | ZHANG Yi LING Yun CAI Qing-yu DU Dong-yu |
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| Affiliation: | (Dept.of Pharmacy, Navy General Hospital, Beijing 100037, China) |
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| Abstract: | OBJECTIVE： To establish the quality standard of Yanyan granules of concentrated sugar- free type. METH- ODS： Scrophularia ningpoensis, Menispermum dauricum , Radix et Rhizoma Glycyrrhizae in the granules were identified by TLC,and the content of linarin in Yanyan granules were determined by HPLC. RESULTS：The TLC spots were clear with high resolution .The linear range of linarin was 4.64-69.6μg（ r = 0.999 9） and the average recovery rate was 98.65% （RSD = 0.79%, n = 6）. CONCLUSION：The established standard is suitable for the quality control of the Yanyan granules of concentrated sugar- free type. |
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| Keywords: | Yanyan granules of concentrated sugar- free type TLC HPLC Quality standard |
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