| 参芍颗粒中芍药苷的含量测定 |
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| 引用本文： | 陈勇敢,王荔. 参芍颗粒中芍药苷的含量测定[J]. 河南大学学报(医学版), 2003, 22(4): 26-27 |
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| 作者姓名： | 陈勇敢 王荔 |
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| 作者单位： | 河南大学药学院,药剂研究室,河南,开封,475001;河南大学药学院,药剂研究室,河南,开封,475001 |
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| 摘 要： | 目的 :建立测定参芍颗粒中芍药苷含量的方法方法 :采用薄层扫描法 ,氯仿 -甲醇 (3∶1)为展开剂 ,5 %香草醛硫酸溶液为显色剂 ,检测波长 2 5 4nm。结果 :芍药苷在 4 μg～ 12 μg范围内 ,浓度与峰面积呈良好的线性关系 ,r=0 .9992 ;平均回收率为 98.73%。结论 :该方法简便、准确 ,可作为参芍颗粒的质控方法
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| 关 键 词： | 芍药苷 参芍颗粒 薄层扫描 |
| 文章编号： | 1008-2867(2003)04-0026-02 |
| 修稿时间： | 2003-07-20 |
Determination of Paeoniflorin in Shenshao Granules |
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| CHEN Yong-gan,WANG Li. Determination of Paeoniflorin in Shenshao Granules[J]. Journal of Henan University, 2003, 22(4): 26-27 |
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| Authors: | CHEN Yong-gan WANG Li |
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| Abstract: | Objective: To establish the determinable method of Paeoniflorin in Shenshao Granules.Methods: CAMAGⅡTLC-scanning was selected ,using chloroform-ethanol(3∶1)as the developing system,the detection wavelength was 254nm.Results: The calibration curve was linear in the range of 4～12μg for Paeoniflorin . The average recovery was 99.78%(r=0.9992).Conclusion: This method is simple and accurate and can be the methods for quality control of Shenshao Granules. |
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| Keywords: | Paeoniflorin Shenshao Granules TLC-scanning |
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