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用示波极谱滴定法测定朴尔敏的含量
引用本文:梁云爱 林乐文. 用示波极谱滴定法测定朴尔敏的含量[J]. 华西药学杂志, 1990, 5(3): 142-144
作者姓名:梁云爱 林乐文
作者单位:山东莒县药品检验所山东医科大学,山东莒县药品检验所山东医科大学,山东诸城市药检所,山东青州卫生学校 济南,济南
摘    要:
本文报道采用示波极谱滴定法,在含1.0g KCl的水溶液中,用0.05mol/L NaOH标准液对朴尔敏及其制剂进行滴定,以示波极谱图的切口出现指示终点。该法操作简便、迅速,平均回收率为100.3%,CV%=0.21‰(n=8)。

关 键 词:朴尔敏 示波极谱滴定 含量测定

DETERMINATION OF CHLORPHENAMINI MALEAS BY OSCILLOPOLAROGRAPHIC TITRATION
Liang Yunai,Lin Lewen,Fan Cunhua,Ma Quanhua Shandong Juxian Institute for Drug Control Shandong Medical University Jinan. DETERMINATION OF CHLORPHENAMINI MALEAS BY OSCILLOPOLAROGRAPHIC TITRATION[J]. West China Journal of Pharmaceutical Sciences, 1990, 5(3): 142-144
Authors:Liang Yunai  Lin Lewen  Fan Cunhua  Ma Quanhua Shandong Juxian Institute for Drug Control Shandong Medical University Jinan
Affiliation:Liang Yunai;Lin Lewen;Fan Cunhua;Ma Quanhua Shandong Juxian Institute for Drug Control 276500 Shandong Medical University Jinan 250012
Abstract:
Here tries the titra-tion of oscilloscope polarogram. That isin the content 1.0g kCl water solution,to use 0.05 mol/L NaOH in raw chlorp-henamini maleas and its preparationdirectly instead of indicator. With thebreak appearing on the oscillosco-pe polarogram picture, that indicatesthe end of the titration. Its result willbe very accurate. The average rate ofrecovery is 100.3% ev%=0.21 (n=8).And the destination is sudio-visual, themanipulation is simple, swift and sens-itive.
Keywords:oscillopolarographic titration  chlorphenamini maleas
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