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凉血散瘀合剂的质量标准
引用本文:吴舜芳,洪美华. 凉血散瘀合剂的质量标准[J]. 中国药师, 2011, 14(1): 47-49
作者姓名:吴舜芳  洪美华
作者单位:1. 佛山市中医院,广东佛山,528000
2. 广东省汕尾市药品检验所
摘    要:
目的:制定凉血散瘀合剂的质量标准。方法:采用薄层色谱法对方中赤芍、栀子进行定性鉴别;采用高效液相色谱法测定丹参中丹酚酸B的含量。结果:所采用的薄层色谱鉴别方法专属性强,阴性对照无干扰;平均回收率100.1%,RSD为0.8%。结论:所建立的方法简便、准确、专属性、重复性好,可作为该制剂的质量控制。

关 键 词:凉血散瘀合剂  薄层色谱法  高效液相色谱法  丹酚酸B  质量标准

Study on Quality Standard of Liangxue Sanyu Mixture
Wu Shunfang,Hong Meihua. Study on Quality Standard of Liangxue Sanyu Mixture[J]. China Pharmacist, 2011, 14(1): 47-49
Authors:Wu Shunfang  Hong Meihua
Affiliation:Wu Shunfang~1,Hong Meihua~2(1.Guangdong Province Foshan Chinese Medicine Hospital,Guangdong Foshan 528000,China,2. Guangdong Province Shanwei Institute for Drug Control)
Abstract:
Objective:To establish quality standard for liangxue sanyu mixture.Method:The Herbaceous peony and Gardenia were identified by TLC,and the content of saivianolic acid B was determined by HPLC.Result:The spots in the TLC were clear and distinguished well,and the average recovery was 100.1%with RSD of 0.8%.Conclusion:The method is simple,accurate and specific. It can be used for the quality control of the preparation.
Keywords:Liangxue sanyu mixture  TLC  HPLC  Salvianolic acid B  Quality standard  
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