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| HPLC法测定舒胃丸中芍药苷含量 | |
| 引用本文： | 刘晋仙,印成霞. HPLC法测定舒胃丸中芍药苷含量[J]. 齐鲁药事, 2010, 29(9): 532-534 |
| 作者姓名： | 刘晋仙 印成霞 |
| 作者单位： | 东营市药品检验所,山东,东营,257091 |
| 摘 要： | 目的建立舒胃丸中芍药苷的高效液相色谱法含量测定方法。方法选用ODSC18色谱柱;以乙腈-水-磷酸(15∶85∶0.05)为流动相;检测波长:230nm;柱温:室温;流速:1.0mL·min-1。结果芍药苷在1.042～5.210μg范围内线性关系良好(r=0.9996),平均回收率为98.77%,RSD=1.28%(n=5)。结论本方法准确,简便,灵敏,可靠,可用于该制剂的质量控制。 |
| 关 键 词： | 舒胃丸 芍药苷 高效液相色谱法 |
Determination of paeoniflorin in Shuwei Pill by HPLC |
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| LIU Jin-xian,YIN Cheng-xia. Determination of paeoniflorin in Shuwei Pill by HPLC[J]. qilu pharmaceutical affairs, 2010, 29(9): 532-534 | |
| Authors: | LIU Jin-xian YIN Cheng-xia |
| Affiliation: | (Dongying Institute for Drug Control,Dongying 257091) |
| Abstract: | OBJECTIVE To establish a method for determining the content of paeoniflorin in Shuwei Pill.METHODS ODS C18 column was adopted in the study.A mixture of acetonitrile-water-phosphoric acid（15∶85∶0.05）served as the mobile phase with a flow rate of 1.0mL·min-1.The detection wavelength was 230nm and column temperature was room temperature.RESULTS The linear range of paeoniflorin was 1.042～5.210μg,r=0.9996.The average rate of recovery was 98.77%,RSD=1.28%（n=5）.CONCLUSION This method was accurate,sample sensitive and reliable and it can be use as the quality control of Shuwei Pill. |
| Keywords: | Shuwei Pill Paeoniflorin HPLC |
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