火焰原子吸收法快速测定食品用橡胶制品中溶出锌 |
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引用本文: | 吕英华,支红峰,杨柳桦,单燕莉,孙烨.火焰原子吸收法快速测定食品用橡胶制品中溶出锌[J].江西医学检验,2011(4):375-376. |
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作者姓名: | 吕英华 支红峰 杨柳桦 单燕莉 孙烨 |
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作者单位: | 浙江省永康市疾病预防控制中心; |
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摘 要: | 目的建立火焰原子吸收法快速测定食品用橡胶制品中溶出锌含量的方法。方法取4%冰乙酸浸泡液直接用火焰原子吸收法测定其锌含量。结果 0.1~2.0mg/L范围内线性良好,相关系数为0.9998,方法检出限为0.0084mg/L。试样测定的相对标准偏差均小于2%(n=6),回收率在95.0~103.8%之间。结论本方法操作简便快速,灵敏度高,结果准确可靠,适于实验室进行食品用橡胶制品中锌的测定。
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关 键 词: | 橡胶制品 锌 原子吸收 测定 |
Rapid determination of zinc released from food contact rubber products by flame atomic absorption spectrometry |
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Institution: | L Yinghua,ZHI Hongfeng,YANG Liuhua,et al.Yongkang Center for Disease Control and Prevention,Zhejiang Yongkang 321300,China |
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Abstract: | Objective To establish a method for determing zinc released from food contact rubber products.Method Zinc soaked in 4% HAc solution was determined by flame atomic absorption spectrometry.Results The linear relationship performed well in the range of 0.1~2.0mg/L,and with 0.9998 of correlation coefficient,0.0084mg/L of the limit of detection respectively.The relative standard deviation value of the method was less than 2%(n=6) and the recovery ranged from 95.0% to 103.8%.Conclusion This method was simple,rapid and highly sensitive,it is suitable for zinc determination in food contact rubber products. |
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Keywords: | Rubber products Zinc Flame atomic absorption spectrometry Determination |
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