| HPLC法对杏桔合剂中桔梗皂苷D的含量测定研究 |
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| 引用本文： | 芮海波,赵学龙,王文晓,张国花.HPLC法对杏桔合剂中桔梗皂苷D的含量测定研究[J].世界中医药,2015,10(6). |
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| 作者姓名： | 芮海波 赵学龙 王文晓 张国花 |
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| 作者单位： | 1 南京市中医院药剂科,南京,210001; 2 南京中医药大学,南京,210014 |
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| 基金项目： | 南京市中医院青年科研基金课题（编号：2011YJ006） |
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| 摘 要： | 目的:建立杏桔合剂中桔梗皂苷D的含量测定方法，为杏桔合剂的质量控制提供量化参考。方法：采用HPLC方法测定桔梗皂苷D的含量。结果：桔梗皂苷D在0.5～8 μg范围内线性关系良好，回归方程:y=238632x+10382，r=0.9997，加样回收率93.64%，RSD=1.54%。结论：应用HPLC测定杏桔合剂中桔梗皂苷D含量的方法可行，可以作为其质量控制的参考依据。
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| 关 键 词： | 杏桔合剂 桔梗皂苷D 含量 HPLC |
| 收稿时间： | 2014/6/16 0:00:00 |
HPLC Method for Determination of Platycodin D in Apricot Orange Mixture |
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| Rui Haibo,Zhao Xuelong,Wang Wenxiao,Zhang Guohua.HPLC Method for Determination of Platycodin D in Apricot Orange Mixture[J].World Chinese Medicine,2015,10(6). |
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| Authors: | Rui Haibo Zhao Xuelong Wang Wenxiao Zhang Guohua |
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| Institution: | 1 Chinese Hospital of Nanjing, Nanjing 210001, China; 2 Nanjing University of Chinese Medicine, Nanjing 210014, China |
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| Abstract: | To establish content determination method of platycodin D in apricot orange mixture so as to provide quantitative information for quality control of apricot orange mixture.Methods:HPLC was used to determine contents of platycodin D.Results:Platycodin D in the range 0.5 ~ 8ug had good linear relationship, and the regression equation was: y=238632x +10382, r=0.9997, recovery was 93.64%, RSD=1.54%.Conclusion:The method of HPLC to determine Platycodin D in apricot orange mixture is feasible, and it can be used as a reference for its quality control. |
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| Keywords: | Apricot orange mixture Platycodin D Content HPLC |
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