气相色谱法检测复方丹参片中樟脑残留量研究 |
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引用本文: | 魏晓舒,高国英,葛晓莹.气相色谱法检测复方丹参片中樟脑残留量研究[J].中国药品标准,2010,11(4):259-262. |
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作者姓名: | 魏晓舒 高国英 葛晓莹 |
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作者单位: | 江苏省无锡药品检验所,无锡,214021 |
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摘 要: | 目的:建立樟脑残留量定性定量方法,了解目前复方丹参片中樟脑残留量情况。方法:以气相色谱双柱法定性,以供试品中樟脑冰片峰面积百分比定量。结果:通过对22批复方丹参片的定性检测:均有樟脑残留量存在,对13批定量推测,樟脑占冰片的面积百分含量为0.19%-1.15%。结论:樟脑冰片面积百分比法能有效用于复方丹参片中樟脑残留量判断。
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关 键 词: | 复方丹参片 樟脑残留量 气相色谱双柱法 |
Study on the Determination of Camphor Residual in Compound Danshen Tablets by Gas Chromatography |
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Authors: | Wei Xiao-shu Gao Guo-ying and Ge Xiao-ying |
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Institution: | (Wuxi Institute of Drug Control of Jiangsu Province, Wuxi 214021 ) |
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Abstract: | Objective:To establish the method for the qualitative and quantitative analysis in order to know Camphor residual in Compound Danshen Tablets at present. Methods: Qualitative analysis by GC method of double column and quantitative analysis by peak area percentage of camphor together with borneol. Results: Compound Danshen tablets all have camphor residual. The residual range was 0. 19%- 1.15% in accordance with peak area percentage. Conclusion:The method of peak area percentage of camphor together with borneol was valuable for the analysis of camphor residual in compound Danshen tablets. |
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Keywords: | compound Danshen tablets camphor residual GC method of double column peak area percentage |
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