| HPLC测定不同厂家参麦注射液中人参皂苷Rg1和Re的含量 |
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| 引用本文： | 马静,李学林,唐进法,孟祥乐.HPLC测定不同厂家参麦注射液中人参皂苷Rg1和Re的含量[J].中国实验方剂学杂志,2013,19(11):79-81. |
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| 作者姓名： | 马静 李学林 唐进法 孟祥乐 |
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| 作者单位： | 河南中医学院第一附属医院药学部,郑州,450000 |
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| 基金项目： | "十一五"国家科技支撑计划项目(2006038086056);河南省重点科技攻关计划项目(10210231007) |
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| 摘 要： | 目的:建立用高效液相色谱法同时测定不同厂家参麦注射液中人参皂苷Rg1和Re的含量.方法:Agilent Eclipse XDB-C18色谱柱(4.6 mm×150 mm,5μm),流动相乙腈-水(19∶81),检测波长203 nm,流速1 mL· min-1,柱温30℃,进样量20 μL.结果:人参皂苷Rg1和人参皂苷Re分别进样量在0.086～4.296 μg(r=0.999 9),0.050 ～2.480 μg(r =0.999 8)与峰面积呈良好的线性关系;人参皂苷Rg1回收率为99.7％ (RSD 1.11％),人参皂苷Re回收率为100.0％ (RSD 1.32％).结论:该方法简便、快速、准确、灵敏度高,可用于参麦注射液的含量测定.
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| 关 键 词： | 高效液相色谱 参麦注射液 人参皂苷Rg1 人参皂苷Re |
| 收稿时间： | 2011/12/26 0:00:00 |
Determination of Ginsenoside Rg1 and Re in Shenmai Injection of Different Manufacturers by HPLC |
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| MA Jing,LI Xue-lin,TANG Jin-fa and MENG Xiang-le.Determination of Ginsenoside Rg1 and Re in Shenmai Injection of Different Manufacturers by HPLC[J].China Journal of Experimental Traditional Medical Formulae,2013,19(11):79-81. |
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| Authors: | MA Jing LI Xue-lin TANG Jin-fa and MENG Xiang-le |
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| Institution: | First Affiliated Hospital of Henan College of Traditional Chinese Medicine, Zhengzhou 450000, China;First Affiliated Hospital of Henan College of Traditional Chinese Medicine, Zhengzhou 450000, China;First Affiliated Hospital of Henan College of Traditional Chinese Medicine, Zhengzhou 450000, China;First Affiliated Hospital of Henan College of Traditional Chinese Medicine, Zhengzhou 450000, China |
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| Abstract: | |
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| Keywords: | HPLC Shenmai injection ginsenoside Rg1 ginsenoside Re |
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