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| 扶正排毒颗粒中小檗碱含量测定 | |
| 引用本文： | 林源,张成中. 扶正排毒颗粒中小檗碱含量测定[J]. 亚太传统医药, 2013, 0(12): 32-33 |
| 作者姓名： | 林源 张成中 |
| 作者单位： | [1]温岭市中医院,浙江温岭317500 [2]阜阳市食品药品检验所,安徽阜阳236015 |
| 摘 要： | 目的：建立扶正排毒颗粒中小檗碱含量的高效液相色谱测定方法。方法：采用DIONEXAc—claim@120C18柱（5tLm120A4．6mm×250mm）；流动相为乙腈-0．05MKH2POt溶液（72：28）；流速为1．0mL／min；检测波长为345nm。结果：在选定色谱条件下，小檗碱在0．1976～0．988μg范围内线性关系良好，样品平均回收率为100．9％，RSD值为1．09％（n=6）。结论：该方法测定简便，结果准确，适用于扶正排毒颗粒中小檗碱的含量测定。 |
| 关 键 词： | 扶正排毒颗粒 小檗碱 高效液相色谱法 |
Determination of Berberine in Fuzhengpaidu granula |
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| Lin Yuan,Zhang Chengzhong. Determination of Berberine in Fuzhengpaidu granula[J]. Asia-Pacific Traditional Medicine, 2013, 0(12): 32-33 | |
| Authors: | Lin Yuan Zhang Chengzhong |
| Affiliation: | 1. Wenling Hospital of Traditional Chinese Medicine, Zhejiang 317500,China 2. Fuyang Institute for Food and Drug Control, Anhui 236015, China) |
| Abstract: | Objective：To develop an HPLC methed for determination berberine in Fuzhengpaidu granula. Methods： A DIONEX Acclaim 120 C18 column（5μm 120A 4.6× 250mm）was used with acetonitrile -0.05M KH2PO4 （72 ： 28）as the mobile phase, the detective wavelength was 345nm. Results： The good liner relationship was obtained under the optimum chromatographic conditions. The average recovery was 100.9 %, RSD was 1.09% （n= 6）. Conclusion： The method is convenient and accurate. It is suitable for qulity control of berberine in Fuzhengpaidu granula. |
| Keywords: | Fuzhengpaidu Granula Berberine HPLC |
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