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| HPLC法测定补肾生精丸中芍药苷的含量 | |
| 引用本文： | 丁广军. HPLC法测定补肾生精丸中芍药苷的含量[J]. 中国中医药现代远程教育, 2011, 9(13): 144-144. DOI: 10.3969/j.issn.1672-2779.2011.13.098 |
| 作者姓名： | 丁广军 |
| 作者单位： | 河南省商丘市第一人民医院,商丘,476100 |
| 摘 要： | 目的建立HPLC法测定补肾生精丸中芍药苷含量的方法。方法采用EclipseXDB-C18色谱柱,乙腈:0.1%磷酸溶液(14:86)为流动相;流速1.0ml·min-1;检测波长230nm。结果芍药苷在0.1332～1.1988μg范围内线性关系良好(r=0.9994),平均回收率为98.26%,RSD=1.29%(n=6)。结论本方法操作简便,专属性强,结果准确,可用于补肾生精丸的质量控制。 |
| 关 键 词： | 芍药苷 高效液相色谱法 含量测定 |
HPLC Determination of Paeoniforin in Bushenshengjing Pill |
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| Ding Guang jun. HPLC Determination of Paeoniforin in Bushenshengjing Pill[J]. Chinese Medicine Modern Distance Education of China, 2011, 9(13): 144-144. DOI: 10.3969/j.issn.1672-2779.2011.13.098 | |
| Authors: | Ding Guang jun |
| Affiliation: | Ding Guang jun Shangqiushi the first people's hospital(476000) |
| Abstract: | Objective To establish a HPLC method to determination of paeoniforin in bushenshengjing pill.Method The chromatographic system consisted of C18 column,using acetonitrile-0.1% phosphate solution（14：86） as mobile phase.The contentwas detected at a waveleng of 230 nm,the flow rate was 1.0ml？min-1.Results The paeoniforin have a good tincar rolatim in the range of 0.1332～1.1988μg（r=0.9994）,the average recovery was 98.26% and RSD=1.29%（n=6）.Conolusion The established method is accuracy,sensitive and simple.It can be used for quality control of bushenshengjing pill. |
| Keywords: | Paeoniforin HPLC Determination |
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