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气相色谱法测定松籽油中γ-亚麻酸的含量
引用本文:陈雅,孟德胜,吴畏,杨征. 气相色谱法测定松籽油中γ-亚麻酸的含量[J]. 中国药房, 2006, 17(5): 377-378
作者姓名:陈雅  孟德胜  吴畏  杨征
作者单位:第三军医大学大坪医院药学部,重庆市,400042
摘    要:
目的建立以气相色谱法测定松籽油中γ-亚麻酸含量的方法。方法色谱柱为5%DEGS柱,检测器温度为220℃,载气为氮气,流速为30ml/min。结果γ-亚麻酸检测浓度在1.162~5.81mg/ml范围内线性关系良好(r=0.9995);平均回收率为97.95%(RSD=0.89%,n=3)。结论该法灵敏、准确、可靠,适用于松籽油中γ-亚麻酸的含量测定。

关 键 词:气相色谱法  松籽油  γ-亚麻酸  含量测定
文章编号:1001-0408(2006)05-0377-02
收稿时间:2005-05-19
修稿时间:2005-07-31

Content Determination of γ-Linoleic Acid in Songzi Oil by Gas Chromatography
CHEN Ya,MENG Desheng,WU Wei,YANG Zheng. Content Determination of γ-Linoleic Acid in Songzi Oil by Gas Chromatography[J]. China Pharmacy, 2006, 17(5): 377-378
Authors:CHEN Ya  MENG Desheng  WU Wei  YANG Zheng
Affiliation:Dept .of Pharmacy, Daping Hospital, The Third Military Medical Universi,y, Chongqing 400042, China
Abstract:
OBJECTIVE:To establish the gas chromatography(GC) for the content determination of γ-linolenic acid in songzi oil.METHODS:The separation was performed on 5% DEGS column with detector temperature at 220℃ and flow rate at 30ml/min,nitrogen gas was used as carrier.RESULTS:The linear range for γ-linoleic acid was 1.162~5.81mg/ml(r= 0.9 995).The average recovery was 97.95%(RSD=0.89%,n=3).CONCLUSION:This method was sensitive,accurate and reliable and suitable for the assaying of γ-linoleic acid in songzi oil.
Keywords:Gas chromatography  Songzi oil  γ-linolenic acid  Content determination
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