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肾衰丸中大黄素的含量测定
引用本文:王虎,陈华庭,徐楚鸿. 肾衰丸中大黄素的含量测定[J]. 中国医院药学杂志, 2005, 25(9): 833-835
作者姓名:王虎  陈华庭  徐楚鸿
作者单位:华中科技大学同济医学院附属协和医院,湖北,武汉,430022
摘    要:
目的:控制肾衰丸的质量,以保证用药安全有效.方法:用高效液相色谱法对大黄素进行含量测定.结果:大黄素加样回收率为98.86%,RSD为1.73%(n=5),3批样品中大黄素的含量分别为0.412,0.407,0.396 mg/粒.结论:本方法简便,快速,结果可靠,可作为肾衰丸的质量控制手段.

关 键 词:大黄素  高效液相色谱  肾衰丸
文章编号:1001-5213(2005)09-0833-03
收稿时间:2004-10-06
修稿时间:2004-10-06

Determination of emodin in Shenshuai pills by RP-HPLC
WANG Hu,CHEN Hua-ting,XU Chu-hong. Determination of emodin in Shenshuai pills by RP-HPLC[J]. Chinese Journal of Hospital Pharmacy, 2005, 25(9): 833-835
Authors:WANG Hu  CHEN Hua-ting  XU Chu-hong
Abstract:
OBJECTIVE To control the quality standard and guarantee the effective and safe use of Shenshuai pills. METHODS Emodin of Shenshuai pills was determined by HPLC. RESULTS Average recovery was 98.86% with RSD of 1.73%. The contents of Shenshuai pills in three batches were 0. 412, 0. 407, 0. 396 mg/pill respectively. CONCLUSION The method is simple, reliable and can be used for controlling the quality of Shenshuai pills.
Keywords:emodin   HPLC   Shenshuai pill
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