| HPLC法测定三七丹参颗粒中的人参皂苷Rg1及Rb1含量 |
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| 引用本文： | 孟庆辉. HPLC法测定三七丹参颗粒中的人参皂苷Rg1及Rb1含量[J]. 中医药学报, 2010, 38(2): 108-109 |
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| 作者姓名： | 孟庆辉 |
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| 作者单位： | 哈药集团世一堂制药厂,黑龙江,哈尔滨,150000 |
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| 基金项目： | 黑龙江省科技攻关项目 |
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| 摘 要： | 目的：运用HPLC法建立三七丹参颗粒中的人参皂苷Rg1及Rb1含量测定方法。方法：采用ZORBAXNH2（4.6nm×150nm）流动相为乙腈：0.1%H3PO4（82：18）;流速为0.8mm·min-1,检测波长为203nm。结果：该法回收率为人参Rg1为99.73%,RSD为0.6%,人参Rb1为99.52%RSD为0.4%。结论：本法操作简单,准确,为测定三七丹参颗粒中人参皂苷Rg1和Rb1的含量提供了可靠的方法。
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| 关 键 词： | 三七丹参颗粒 人参皂苷Rg1 人参皂苷Rb1 HPLC |
Determination of Gensenoside Rg1 and Rb1 in Sanqidanshen Granule by HPLC |
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| MENG Qing-hui. Determination of Gensenoside Rg1 and Rb1 in Sanqidanshen Granule by HPLC[J]. Acta Chinese Medicine and Pharmacology, 2010, 38(2): 108-109 |
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| Authors: | MENG Qing-hui |
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| Affiliation: | MENG Qing-hui (Shiyitang Pharmaceutical factory of Harbin Pharmaceutical ) |
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| Abstract: | Objection：To establish a method for determination of GensenosideRg1 and Rb1 in Sanqidanshen Granule by HPLC Methods： The determination was carried out with ZORBAXNH2 column （4. 6nm × 150nm） using methanol-water （82：18）as thw mobile plase at a flow rate of 0. 8ml/min and detected at the wave longth 203nm . Result：The recovery of this method in GensenosideRg1 was 99. 37% RSD was 0. 6% ;in GensenosideRb1 was 99. 52% RSD was 0. 40% . Conclusion：The method was simple and accurate and could bs used to Determination of GensenosideRg1 and Rb1in Sanqidanshen keli . |
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| Keywords: | HPLC |
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