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| 怀牛膝水溶性化学成分研究 | |
| 引用本文： | 汪涛,崔书亚,索有瑞,鲁润华. 怀牛膝水溶性化学成分研究[J]. 中国中药杂志, 2004, 29(7): 649-652 |
| 作者姓名： | 汪涛 崔书亚 索有瑞 鲁润华 |
| 作者单位： | 1. 中国科学院,兰州化学物理研究所,甘肃,兰州,730000 2. 兰州大学,化学化工学院,甘肃,兰州,730000 3. 中国科学院,兰州化学物理研究所,甘肃,兰州,730000;中国科学院,西北高原生物研究所,青海,西宁,810001 |
| 摘 要： | 目的 :研究河南省武陟县怀牛膝水溶性部分的化学成分。方法 :色谱等方法分离纯化 ,理化性质和光谱方法鉴定化学成分。结果 :分离并鉴定了 7个化合物 ,分别为正丁基吡喃果糖苷 (Ⅰ ) ,尿囊素 (Ⅱ ) ,齐墩果酸(Ⅲ ) ,3-O-(β-D 吡喃葡萄糖醛酸 ) 齐墩果酸 -28-O-(β-D-吡喃葡萄糖 ) (Ⅳ ) ,蜕皮甾酮 (Ⅴ ) ,谷氨酸 (Ⅵ ) ,3-O-(β-D-吡喃葡萄糖 ) 齐墩果酸-28-O-(β-D-吡喃葡萄糖 ) (Ⅶ )。 结论 :Ⅲ～Ⅶ化合物为首次自该植物中分离得到。 |
| 关 键 词： | 怀牛膝 三萜皂苷 齐墩果酸 |
| 文章编号： | 1001-5302(2004)07-0649-04 |
| 收稿时间： | 2004-01-05 |
Studies on water-soluble chemical constituents in root of Achyranthes bidentata |
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| WANG Tao;CUI Shu-ya;SUO You-rei;LU Run-hua. Studies on water-soluble chemical constituents in root of Achyranthes bidentata[J]. China Journal of Chinese Materia Medica, 2004, 29(7): 649-652 | |
| Authors: | WANG Tao CUI Shu-ya SUO You-rei LU Run-hua |
| Affiliation: | Lanzhou Institute of Chemical and Physics, Chinese Academy of Science, Lanzhou 730000, China. |
| Abstract: | OBJECTIVE: To study the water-soluble chemical constituents in root of Achyranthes bidentata. METHOD: The chemical constituents were isolated by silica gel column chromatography and the structures were elucidated by the NMR spectra and physico-chemical properties. RESULT: Seven compounds were obtained and identified as n-butyl-beta-D-fructopyranoside (I), oleanoic acid (II), 3-O-[beta-D-glucopyranosyl], oleanoic acid 28-O-beta-D-glucopyranoside (III), allantoin (IV), 20-hydroxy ecdysone (V), glutamic acid (VI), 3-O-[beta-D-glucopyranosyl], oleanoic acid 28-O-beta-D-glucopyranosyl ester (VII). CONCLUSION: Compounds III-VII were obtained from this plant for the first time. |
| Keywords: | Achyranthes bidentata achybidensaponin triterpene saponin |
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