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裸花紫珠叶中1个新的环烯醚萜苷
引用本文:马员宇,付辉政,潘蕾,王杰,周志强,黄波,罗跃华. 裸花紫珠叶中1个新的环烯醚萜苷[J]. 中草药, 2018, 49(8): 1746-1750
作者姓名:马员宇  付辉政  潘蕾  王杰  周志强  黄波  罗跃华
作者单位:南昌大学药学院;江西省药品检验检测研究院江西省药品与医疗器械质量工程技术研究中心
基金项目:国家自然科学基金资助项目(81373955);江西省自然科学基金资助项目(20142BAB205085);校级创新基金(CX2016291)
摘    要:目的研究裸花紫珠Callicarpa nudiflora的化学成分。方法利用硅胶、MPLC柱色谱、高效制备液相色谱等色谱方法进行分离纯化,根据理化常数测定及波谱数据分析鉴定化合物结构。结果从裸花紫珠叶80%乙醇提取物中分离得到5个化合物,分别鉴定为6′-O-咖啡酰基益母草苷(1)、木犀草素(2)、5,4′-二羟基-3,7,3′-三甲氧基黄酮(3)、木犀草素-4′-O-(6″-E-咖啡酰)-β-D-吡喃葡萄糖苷(4)、2α,3α,19α,23-四羟基-12-烯-28-乌苏酸(5)。结论化合物1为新化合物,命名为裸花紫珠苷A1。

关 键 词:裸花紫珠  环烯醚萜苷  6''-O-咖啡酰基益母草苷  裸花紫珠苷A1  木犀草素  5, 4''-二羟基-3, 7, 3''-三甲氧基黄酮
收稿时间:2017-12-04

A new iridoid glycoside from leaves of Callicarpa nudiflora
MA Yuan-yu,FU Hui-zheng,PAN Lei,WANG Jie,ZHOU Zhi-qiang,HUANG Bo and LUO Yue-hua. A new iridoid glycoside from leaves of Callicarpa nudiflora[J]. Chinese Traditional and Herbal Drugs, 2018, 49(8): 1746-1750
Authors:MA Yuan-yu  FU Hui-zheng  PAN Lei  WANG Jie  ZHOU Zhi-qiang  HUANG Bo  LUO Yue-hua
Affiliation:Jiangxi Center for Drug Evaluation, Nanchang 330006, China;Jiangxi Provincial Institute for Drug Control, Jiangxi Provincial Engineering Research Center for Drug and Medical Device Quality, Nanchang 330029, China,Jiangxi Provincial Institute for Drug Control, Jiangxi Provincial Engineering Research Center for Drug and Medical Device Quality, Nanchang 330029, China,Jiangxi Provincial Institute for Drug Control, Jiangxi Provincial Engineering Research Center for Drug and Medical Device Quality, Nanchang 330029, China,Jiangxi Provincial Institute for Drug Control, Jiangxi Provincial Engineering Research Center for Drug and Medical Device Quality, Nanchang 330029, China,Jiangxi Provincial Institute for Drug Control, Jiangxi Provincial Engineering Research Center for Drug and Medical Device Quality, Nanchang 330029, China,Jiangxi Provincial Institute for Drug Control, Jiangxi Provincial Engineering Research Center for Drug and Medical Device Quality, Nanchang 330029, China and Jiangxi Provincial Institute for Drug Control, Jiangxi Provincial Engineering Research Center for Drug and Medical Device Quality, Nanchang 330029, China
Abstract:
Keywords:Callicarpa nudiflora Hook. et Arm.  iridoid glycosides  6''-O-caffeoyl-ajugol  nudifloside A1  luteolin  5, 4''-dihydroxy-3, 7, 3''-trimethoxyflavone
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