| 愈肝灵胶囊的制备与质量控制 |
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| 引用本文： | 居靖,王曙光. 愈肝灵胶囊的制备与质量控制[J]. 中国现代应用药学, 2010, 27(6): 510-512 |
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| 作者姓名： | 居靖 王曙光 |
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| 作者单位： | 1.安徽医科大学附属安庆医院，安徽 安庆246003；2.安徽中医学院，合肥230061 |
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| 摘 要： | 目的研究愈肝灵胶囊制备与质量控制的方法。方法采用薄层色谱法对愈肝灵胶囊中的博落回进行定性鉴别;以HPLC对制剂中的白屈菜红碱进行含量测定。结果薄层色谱清晰,无干扰,重复性良好;白屈菜红碱在0.1048～0.6289μg·mL^-1内呈良好的线性关系,回收率达到99.50%,RSD=1.45%。结论该方法准确度高,重复性好,简便快捷,可作为愈肝灵胶囊的质量控制指标。
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| 关 键 词： | 愈肝灵胶囊 制备 质量控制 |
Preparation and Quality Control of Yuganling Capsule |
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| JU Jing,WANG Shuguang. Preparation and Quality Control of Yuganling Capsule[J]. The Chinese Journal of Modern Applied Pharmacy, 2010, 27(6): 510-512 |
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| Authors: | JU Jing WANG Shuguang |
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| Affiliation: | 1. Anqing Affiliated Hopistal of Anhui Medical University, Anqing 246003, China; 2. Anhui college of TCM, Hefei 230061, China |
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| Abstract: | OBJECTIVE To study the formulation and preparation procedure of Yuganling capsule and develop an HPLC method for the content determination.METHODS Plumepoppy was identified by TLC,and chelerythrine was determined by HPLC.RESLUTS TLC spots developed were fairly clear,and the blank test showed no interference.Chelerythrine showed a good linear relationship in the range of 0.1048-0.6289 μg·mL^-1 and the average recovery was up to 99.50%,RSD was 1.45%.CONCLUSION The method is accurate,reproducible,simple,and can be used as the quality control of this preparation. |
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| Keywords: | Yuganling capsule preparation quality control |
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