| 乳结消散片中丹参酮ⅡA的含量测定 |
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| 引用本文： | 杨毅恒,张晓乐,王淑庆,严宝霞. 乳结消散片中丹参酮ⅡA的含量测定[J]. 中国药学杂志, 2001, 36(1): 56-57 |
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| 作者姓名： | 杨毅恒 张晓乐 王淑庆 严宝霞 |
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| 作者单位： | 北京医科大学附属第三医院药剂科, |
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| 摘 要： | 目的建立高效液相色谱法测定丹参酮ⅡA含量的方法。方法C18柱以甲醇-水(70:30)作为流动相,检测波长269nm。结果丹参酮ⅡA浓度在0～33ng·Ml-1范围内,峰面积与进样量线形关系良好,回归方程Y=9725X-2584,r=0.9997。平均回收率为98.29%,RSD=1.86%。结论本法重现性好,准确快速,可作为质量控制指标。
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| 关 键 词： | 丹参酮ⅡA 高效液相色谱法 含量测定 |
| 文章编号： | 1001-2494(2001)01-0056-02 |
| 收稿时间： | 1999-12-24; |
| 修稿时间： | 1999-12-24 |
Determination oftanshinone |
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| YANG Yi-heng,ZHANG Xiao-le,WANG Shu-qing,YAN Bao-xia. Determination oftanshinone[J]. Chinese Pharmaceutical Journal, 2001, 36(1): 56-57 |
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| Authors: | YANG Yi-heng ZHANG Xiao-le WANG Shu-qing YAN Bao-xia |
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| Affiliation: | Department of Pharmacy,The third school of Clinical medicine,Beijing University,Beijing 100083,China |
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| Abstract: | OBJECTIVE To develope an HPLC assay for the determination of tanshinoneⅡA.METHOD C18ODS column was used.The mobile phase was consisted of MeOH-water(70∶30).The detection wavelength was at 269 nm.RESULT The linear regression equation was Y=9725X-2584,r=0.9997.The average recovery was 98.29% with RSD=1.86%.(n=5).CONCLUSION The method may be used for quality control. |
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| Keywords: | A')" href=" #" >tanshinoneⅡA HPLC detelmination |
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