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黑龙骨化学成分研究
引用本文:李勇,刘云宝,庾石山. 黑龙骨化学成分研究[J]. 中国中药杂志, 2013, 38(10): 1536-1538
作者姓名:李勇  刘云宝  庾石山
作者单位:天然药物活性物质与功能国家重点实验室,中国医学科学院北京协和医学院药物研究所,北京100050
基金项目:国家自然科学基金项目(21132009)
摘    要:
该文对有毒药用植物黑龙骨的化学成分进行了研究.利用大孔吸附树脂、正相和反相硅胶柱和制备型HPLC等色谱技术从中分离得到9个化合物,分别为:东莨菪内酯(1),trans-3,4-methylenedioxycinnamyl alcohol(2),syringaresinol (3),syringaresinol 4-O-β-D-glucopyranoside(4),6 '-O-(E)-feruloylsucrose(5),loliolide(6),4-hydroxy-3-methoxyl-benzaidehyde (7),Δ5-pregnene-3β,17α,20α-triol(8),Δ5-pregnene-3β,17α,20α-triol-20-O-β-D-canaropyranoside (9).并运用质谱、核磁等波谱技术对分离得到的化合物进行了结构鉴定.化合物1,2,5~7为首次从该属植物中分离得到已知化合物.

关 键 词:黑龙骨  杠柳属  化学成分
收稿时间:2013-01-25

Chemical constituents of Periploca forrestii
LI Yong,LIU Yun-bao and YU Shi-shan. Chemical constituents of Periploca forrestii[J]. China Journal of Chinese Materia Medica, 2013, 38(10): 1536-1538
Authors:LI Yong  LIU Yun-bao  YU Shi-shan
Affiliation:State Key Laboratory of Bioactive Substance and Function of Natural Medicines, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China;State Key Laboratory of Bioactive Substance and Function of Natural Medicines, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China;State Key Laboratory of Bioactive Substance and Function of Natural Medicines, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China
Abstract:
Keywords:Periploca forrestii  Periploca genus  chemical constituents
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