| 青蛇藤中的一个新寡糖 |
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| 引用本文： | 龙秀红,徐冉,张援虎,谭小鸿,孙黔云. 青蛇藤中的一个新寡糖[J]. 中国中药杂志, 2012, 37(2): 226-229 |
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| 作者姓名： | 龙秀红 徐冉 张援虎 谭小鸿 孙黔云 |
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| 作者单位： | 1. 贵州大学生命科学学院,贵州贵阳550025;贵州省、中国科学院天然产物化学重点实验室,贵州贵阳550002
2. 贵州省、中国科学院天然产物化学重点实验室,贵州贵阳,550002 |
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| 基金项目： | National Program on Key Basic Research Project (2009CB526512), Traditional Chinese Medicine Modernization Project in Guizhou Province ([2006]5041);Science and Technology Foundation of Guizhou Province ([2006]2090) |
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| 摘 要： | 目的:研究青蛇藤中的化学成分。方法:应用硅胶、Sephadex LH-20,MCI,Rp-18柱色谱进行分离、纯化,根据理化常数和光谱分析鉴定其结构。结果:从青蛇藤氯仿萃取部分分离鉴定了2个寡糖,鉴定为:4-O-acetyl-β-cym(1→4)-O-β-D-cym(1→4)-O-β-D-can(1→4)-O-β-D-cym(l→4)-O-oleandronicacid-δ-lactone(1),和perisaccharide B(2)。结论:化合物1为新化合物,化合物2为首次从该植物中分离得到。
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| 关 键 词： | 青蛇藤 寡糖 |
| 收稿时间： | 2011-04-05 |
A new oligosaccharide from Periploca calophylla |
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| LONG Xiuhong,XU Ran,ZHANG Yuanhu,TAN Xiaohong and SUN Qianyun. A new oligosaccharide from Periploca calophylla[J]. China Journal of Chinese Materia Medica, 2012, 37(2): 226-229 |
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| Authors: | LONG Xiuhong XU Ran ZHANG Yuanhu TAN Xiaohong SUN Qianyun |
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| Affiliation: | College of Life Science, Guizhou University, Guiyang 550025, China;Key Laboratory of Chemistry for Natural Products of Guizhou Province and Chinese Academy of Sciences, Guiyang 550002, China;College of Life Science, Guizhou University, Guiyang 550025, China;Key Laboratory of Chemistry for Natural Products of Guizhou Province and Chinese Academy of Sciences, Guiyang 550002, China;Key Laboratory of Chemistry for Natural Products of Guizhou Province and Chinese Academy of Sciences, Guiyang 550002, China;Key Laboratory of Chemistry for Natural Products of Guizhou Province and Chinese Academy of Sciences, Guiyang 550002, China;Key Laboratory of Chemistry for Natural Products of Guizhou Province and Chinese Academy of Sciences, Guiyang 550002, China |
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| Abstract: | Objective:To study thechemical constituents of Periploca calophylla.Method:Various chromatographic techniques were used to isolate the constituents,and their structures were identified by spectral and chemical methods.Result:Two oligosaccharides were isolated from the chloroform part of P.calophylla and their structures were identified as 4-O-acetyl-β-cymaropyranosyl(1→4)-O-β-D-cymaropyranosyl(1→4)-O-β-D-canaropyranosyl(1→4)-O-β-D-cymaropyranosy(l→4)-O-oleandronic acid-δ-lactone(1),and perisaccharide B(2).Conclusion:Compound 1 is a new com-pound.Compound 2 is reported for the first time from this plant. |
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| Keywords: | Periploca calophylla oligosaccharides |
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