| 高效液相色谱法测定肝心康胶囊中丹参酮Ⅱ_A的含量 |
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| 引用本文： | 苏玉娟,李延雪,隋译.高效液相色谱法测定肝心康胶囊中丹参酮Ⅱ_A的含量[J].中国药房,2006,17(4):296-297. |
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| 作者姓名： | 苏玉娟 李延雪 隋译 |
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| 作者单位： | 黑龙江鸡西市药品检验所,鸡西市,158100 |
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| 摘 要： | 目的:建立以高效液相色谱法测定肝心康胶囊中丹参酮ⅡA含量的方法。方法:色谱柱为C18,流动相为甲醇-水(80∶20),流速为0·8ml/min,检测波长为269nm。结果:丹参酮ⅡA进样量在0·16μg~0·80μg范围内与峰面积积分值线性关系良好(r=0·9989),平均加样回收率为96·3%(RSD=1·21%)。结论:本方法简便、准确、快速、重现性好,可用于本品的质量控制。
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| 关 键 词： | 高效液相色谱 肝心康胶囊 丹参酮Ⅱ_A 含量 |
| 文章编号： | 1001-0408(2006)04-0296-02 |
| 收稿时间： | 08 31 2005 12:00AM |
| 修稿时间： | 10 31 2005 12:00AM |
Determination of Tanshinone Ⅱ A in Ganxinkang Capsules by HPLC |
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| SU Yujuan,LI Yanxue,SUI Yi.Determination of Tanshinone Ⅱ A in Ganxinkang Capsules by HPLC[J].China Pharmacy,2006,17(4):296-297. |
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| Authors: | SU Yujuan LI Yanxue SUI Yi |
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| Institution: | Heilongjiang Jixi Institute for Drug Control,Jixi 158100,China |
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| Abstract: | OBJECTIVE:To establish HPLC method for the determination of tanshinoneⅡ A in Ganxinkang capsules.ME_ THODS:The separation was carried out on C 18 column.The mobile phase was composed of methanol-water(80∶20)with a fl_ ow rate at0.8ml/min and detection wavelength at269nm.RESULTS:The linear range of tanshinoneⅡ A was0.16μg～0.80μg (r=0.9989)with average recovery at96.3%(RSD=1.21%).CONCLUSION:This method was convenient,accurate,rapid and reproducible,and suitable for the quality control of this preparation. |
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| Keywords: | HPLC Ganxinkang capsules TanshinoneⅡ A Content |
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