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海南龙血树茎及其血竭脂溶性成分的气相色谱-质谱联用分析
引用本文:罗应,王辉,左文健,戴好富,梅文莉.海南龙血树茎及其血竭脂溶性成分的气相色谱-质谱联用分析[J].时珍国医国药,2011,22(11):2603-2605.
作者姓名:罗应  王辉  左文健  戴好富  梅文莉
作者单位:1. 海南大学农学院,海南海口570228;中国热带农业科学院热带生物技术研究所海南省黎药资源天然产物研究与利用重点实验室,海南海口571101
2. 中国热带农业科学院热带生物技术研究所海南省黎药资源天然产物研究与利用重点实验室,海南海口571101;海口市热带天然产物研究与利用重点实验室,海南海口571101
基金项目:国家自然科学基金,海南省自然科学基金-,中央级科研院所基本科研业务费专项资金资助项目
摘    要:目的分析海南龙血树茎及其血竭脂溶性成分。方法采用溶剂萃取法提取海南龙血树茎及其血竭脂溶性成分,用GC-MS联用技术鉴定其化学成分。结果从海南龙血树茎及其血竭脂溶性成分中分别鉴定出21和33种成分,海南龙血树茎脂溶性成分主要有邻苯二甲酸二异辛酯(10.33%)和环木菠萝烷醇(8.51%);其血竭脂溶性成分主要有薯蓣皂苷元(10.62%)和7-羟基-4’-甲氧基黄烷(9.88%),其中8个化合物为共有成分。结论海南龙血树茎及其血竭脂溶性成分的组成和含量存在着差异,在入药和研究中都应区别对待。

关 键 词:海南龙血树  血竭  气相色谱-质谱联用  脂溶性成分

GC- MS Analysis for Liposoluble Components in the Stem and Dragon's Blood of Dracaena cambodiana
LUO Ying,WANG Hui,ZUO Wen-jian,DAI Hao-fu,MEI Wen-li.GC- MS Analysis for Liposoluble Components in the Stem and Dragon's Blood of Dracaena cambodiana[J].Lishizhen Medicine and Materia Medica Research,2011,22(11):2603-2605.
Authors:LUO Ying  WANG Hui  ZUO Wen-jian  DAI Hao-fu  MEI Wen-li
Institution:LUO Ying 1,2,WANG Hui 2,3,ZUO Wen-jian 2,DAI Hao-fu 2,MEI Wen-li 2,3* (1.College of Agriculture,Hainan University,Haikou 570228,China,2.Hainan Key Laboratory for Research and Development of Natural Products from Li Folk Medicine,Institute of Tropical Bioscience and Biotechnology,Chinese Academy of Tropical Agricultural Sciences,Haikou 571101,3.Haikou Key Laboratory for Research and Development of Tropical Natural Products,China)
Abstract:Objective To analyze the chemical constituents of liposoluble components in the stem and dragon′s blood of Dracaena cambodiana. Methods The liposoluble components were extracted by solvent method and identified by GC-MS. Results For the first time,twenty-one and thirty-three ingredients were identified from the liposoluble components of the stem and dragon′s blood of D.cambodiana,respectively.The main constituents of liposoluble components of the stem of D.cambodiana were diisooctyl phthalate(10.33%) and cycloartanol(8.51%),while diosgenin(10.62%) and 7-hydroxy-4-methoxyflavan(9.88%) were the main constituents of liposoluble components of its dragon′s blood.Eight ingredients existed in both liposoluble components of stem and dragon′s blood of D.cambodiana. Conclusion The constituents of liposoluble components of the stem of D.cambodiana and its dragon′s blood are different,so they should be dealt with differently in clinical application and research.
Keywords:Dracaena cambodiana  Dragon′s blood  GC-MS  Liposoluble components
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