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| 草珊瑚醋酸乙酯部位化学成分研究 | |
| 引用本文： | 王超,朱丽萍,杨敬芝,李创军,张东明. 草珊瑚醋酸乙酯部位化学成分研究[J]. 中国中药杂志, 2010, 35(6): 714-717 |
| 作者姓名： | 王超 朱丽萍 杨敬芝 李创军 张东明 |
| 作者单位： | 中国医学科学院北京协和医学院药物研究所中草药物质基础与资源利用,教育部重点实验室,北京100050 |
| 基金项目： | 国家自然科学基金项目(20432030,20772157) |
| 摘 要： | 目的:对草珊瑚的化学成分进行分离与鉴定,为研究其活性成分提供参考。方法:利用聚酰胺、正相硅胶、Sepha-dex LH-20柱色谱和HPLC进行化合物的分离与纯化,根据化合物的理化性质和波谱数据进行结构鉴定。结果:从草珊瑚70%乙醇提取物中分离鉴定了9个化合物,分别为:异东莨菪素(1),syringaresinol monoside(2),styraxjaponoside B(3),5-O-caf-feoylshikimic acid(4),shizukanolide E(5),异落新妇苷(6),新异落新妇苷(7),落新妇苷(8),新落新妇苷(9)。结论:化合物1~7为首次从该属植物中分离得到。 |
| 关 键 词： | 草珊瑚 化学成分 |
| 收稿时间： | 2009-07-23 |
Chemical constituents from Sarcandra glabra |
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| WANG Chao,ZHU Liping,YANG Jingzhi,LI Chuangjun and ZHANG Dongming. Chemical constituents from Sarcandra glabra[J]. China Journal of Chinese Materia Medica, 2010, 35(6): 714-717 | |
| Authors: | WANG Chao ZHU Liping YANG Jingzhi LI Chuangjun ZHANG Dongming |
| Affiliation: | Key Laboratory of Bioactive Substances and Resources Utilization of Chinese Herb Medicine, Ministery of Education, Instituent of Materia Medica, Peking Union Medical College Chinese Academy of Medical Sciences, Beijing 100050, China;Key Laboratory of Bioactive Substances and Resources Utilization of Chinese Herb Medicine, Ministery of Education, Instituent of Materia Medica, Peking Union Medical College Chinese Academy of Medical Sciences, Beijing 100050, China;Key Laboratory of Bioactive Substances and Resources Utilization of Chinese Herb Medicine, Ministery of Education, Instituent of Materia Medica, Peking Union Medical College Chinese Academy of Medical Sciences, Beijing 100050, China;Key Laboratory of Bioactive Substances and Resources Utilization of Chinese Herb Medicine, Ministery of Education, Instituent of Materia Medica, Peking Union Medical College Chinese Academy of Medical Sciences, Beijing 100050, China;Key Laboratory of Bioactive Substances and Resources Utilization of Chinese Herb Medicine, Ministery of Education, Instituent of Materia Medica, Peking Union Medical College Chinese Academy of Medical Sciences, Beijing 100050, China |
| Abstract: | Objective: To study the chemical constituents of the plant of Sarcandra glabra and provide reference for the study of the bioactive substances.Method: The compounds were isolated from the EtOH extract by various chromatographic methods and their structures were elucidated by their physico-chemical properties and the analysis of their spectral data.Result: Nine compounds were isolated and identified as isoscopletin(1),syringaresinol monoside(2),styraxjaponoside B(3),5-O-caffeoylshikimic acid(4),shizukanolide... |
| Keywords: | Sarcandra glabra chemical constituents |
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