| 生津润燥合剂质量标准研究 |
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| 引用本文： | 胡敏敏,张敏娟,金卓. 生津润燥合剂质量标准研究[J]. 安徽医药, 2013, 17(3): 391-393 |
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| 作者姓名： | 胡敏敏 张敏娟 金卓 |
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| 作者单位： | 江苏省无锡市中医医院,江苏,无锡,214001;江苏省无锡药品检验所,江苏,无锡,214020 |
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| 摘 要： | 目的对生津润燥合剂进行质量标准建立。方法采用TLC对制剂中玄参、赤芍进行鉴别;采用HPLC对生津润燥合剂中芍药苷进行含量测定。结果用TLC能检出玄参、赤芍,芍药苷在0.002～0.10 g.L-1范围内线性关系良好,r=0.999 6,平均回收率为94.83%,RSD为0.79%。结论该方法可靠,易操作,重现性好,专属性强,可用于控制生津润燥合剂的质量。
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| 关 键 词： | 生津润燥合剂 质量标准 玄参 赤芍 芍药苷 TLC HPLC |
Quality standard study for shengjin runzao heji |
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| HU Min-min , ZHANG Min-juan , JIN Zhuo. Quality standard study for shengjin runzao heji[J]. Anhui Medical and Pharmaceutical Journal, 2013, 17(3): 391-393 |
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| Authors: | HU Min-min ZHANG Min-juan JIN Zhuo |
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| Affiliation: | 1.Wuxi Hospital of Traditional Chinese Medicine,Wuxi 214001,China;2.Wuxi Institute for Drug Control,Wuxi 214020,China) |
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| Abstract: | Objective To establish the quality standard for shengjin runzao heji.Methods TLC was used to identify scrophulariae radix,paeoniae radix rubra;and HPLC was used to determine the content of paeoniflorin.Results The spots in the TLC were clear and distinguished well.The linear range of paeoniflorin was 0.002~0.10 g·L-1（r=0.999 6）.The average recovery was 94.83% with RSD of 0.79%.Conclusion This method is reliable,simple and of good reproducibility and accuracy,so it can be used for quality control of shengjin runzao heji. |
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| Keywords: | shengjin runzao heji quality standard scrophulariae radix paeoniae radix rubra paeoniflorin TLC HPLC |
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