| 独一味滴丸质量控制研究 |
| |
| 引用本文： | 田军,李刘辉,刘永. 独一味滴丸质量控制研究[J]. 安徽医药, 2007, 11(5): 399-400 |
| |
| 作者姓名： | 田军 李刘辉 刘永 |
| |
| 作者单位： | 安徽省药物研究所,安徽省中药研究与开发重点实验室,安徽,合肥,230022;安徽省药物研究所,安徽省中药研究与开发重点实验室,安徽,合肥,230022;安徽省药物研究所,安徽省中药研究与开发重点实验室,安徽,合肥,230022 |
| |
| 摘 要： | 目的 建立独一味滴丸质量标准.方法 采用薄层色谱法对方中独一味进行定性鉴别;采用高效液相色谱法测定木犀草素的含量.结果 供试品斑点显色清晰,阴性对照无干扰.木犀草素的线性范围为0.0275～0.88 μg(r=0.999 9,n=5).平均回收率为100.9%.结论 所建立的定性定量方法专属性强,重复性好,可有效控制该产品质量.
|
| 关 键 词： | 独一味滴丸 薄层色谱法 高效液相色谱法 质量标准 |
| 文章编号： | 24370468 |
| 修稿时间： | 2006-12-11 |
Study on the quality control standard for duyiwei drop pills |
| |
| TIAN Jun,LI Liu-hui,LIU Yong. Study on the quality control standard for duyiwei drop pills[J]. Anhui Medical and Pharmaceutical Journal, 2007, 11(5): 399-400 |
| |
| Authors: | TIAN Jun LI Liu-hui LIU Yong |
| |
| Affiliation: | Anhui Institute of Materia Medica,Hefei 230022,China |
| |
| Abstract: | Aim To establish the quality control standard for duyiwei drop pills. Method Herba lamiophlomis was identified by TLC method. The content of Luteolin in duyiwei drop pills was determined by HPLC. Results The thin layer choromatogram spots were clear without any interference in the blank test. The linear range of luteolin was 0. 0275 - 0.88 ug, r = 0. 999 9. The average recovery was 100. 9%. Conclusion The qualitative and quantitive methods are highly special,sensitive and repeatable,and they can be used for controlling the quality of the duyiwei drop pills. |
| |
| Keywords: | duyiwei drop pills TLC HPLC quality control standard |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
