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β-环糊精包合莪术挥发油的工艺研究
引用本文:李丹,许江,夏顺宁,濮存海,金顺福,刘美辉. β-环糊精包合莪术挥发油的工艺研究[J]. 中药材, 2004, 27(11): 866-869
作者姓名:李丹  许江  夏顺宁  濮存海  金顺福  刘美辉
作者单位:1. 南京市药品检验所,南京,210025
2. 南京中山制药厂,南京,210012
3. 延边大学,延吉,133000
摘    要:目的:研究β-环糊精包合莪术挥发油的最佳工艺.方法:正交实验法,考察挥发油利用率、包合物收率、及包合物含油率3个指标.结果:优选出包合工艺为:挥发油: 环糊精(1: 8),包合温度为80℃,包合时间1 h,挥发油利用率为86%.结论:此工艺可以用于大生产.

关 键 词:莪术挥发油  β-环糊精包合物  正交设计法
修稿时间:2004-04-07

Study on Preparation of β-cyclodextrin Inclusion Volatile Oil from Rhizoma Curcumae
Li Dan ,Xu Jiang ,Xia Shunning ,Pu Cunhai ,Jin Shunfu ,Liu Meihui. Study on Preparation of β-cyclodextrin Inclusion Volatile Oil from Rhizoma Curcumae[J]. Journal of Chinese medicinal materials, 2004, 27(11): 866-869
Authors:Li Dan   Xu Jiang   Xia Shunning   Pu Cunhai   Jin Shunfu   Liu Meihui
Affiliation:Nanjing Institute for Drug Control, Nanjing.
Abstract:OBJECTIVE: To study optimum inclusion process conditions for volatile oil from Rhizoma Curcumae. METHOD: The study was carried out with orthogonal design. The process conditions were studied by determining the utilazision ratio of volatile oil from Rhizoma Curcumae, the oil-bearing rate and extract ratio of inclusion compound. RESULTS: The optimum preparation conditions for inclusion were established as: volatile oil:beta-CD was 1:8, the inclusion temperature was at 80 degrees C and inclusion time for 3 h, ultilizasion rate of volatile oil was 86%. CONCLUSION: The method can be used for mass production.
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