| 反相高效液相色谱法测定维肝福泰胶囊中五味子醇甲的含量 |
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| 引用本文： | 梁静,杨静伟. 反相高效液相色谱法测定维肝福泰胶囊中五味子醇甲的含量[J]. 中国现代药物应用, 2008, 2(24): 52-53 |
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| 作者姓名： | 梁静 杨静伟 |
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| 作者单位： | 梁静(黑龙江省医药工业研究所,150081)；杨静伟(黑龙江省医药工业研究所,150081)； |
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| 摘 要： | 目的建立维肝福泰胶囊（人参茎叶皂苷、五味子醇浸膏、树舌多糖等）中五味子醇甲的含量测定方法。方法采用YMC C18柱,甲醇：0.03%磷酸溶液（65：35）为流动相,检测波长为220 nm。结果五味子醇甲在0.142～1.140μg呈良好的线性范围（r=0.999 7）,平均回收率为99.49,RSD为1.93%。结论该方法简便准确,重现性好,可用于维肝福泰胶囊的质量控制。
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| 关 键 词： | 反相高效液相色谱法 维肝福泰胶囊 五味子醇甲 含量测定 |
Determination of ginsenoside Re、ginsenoside Rg1 and schisandrin in Weiganfutai capsule by RP-HPLC |
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| LIANG Jing,YANG Jing-wei. Determination of ginsenoside Re、ginsenoside Rg1 and schisandrin in Weiganfutai capsule by RP-HPLC[J]. Chinese Journal of Modern Drug Application, 2008, 2(24): 52-53 |
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| Authors: | LIANG Jing YANG Jing-wei |
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| Affiliation: | . (Heilongjiang Institute of Pharmaceutical Industry, Harbin 150081, China) |
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| Abstract: | Objective To establish a HPLC method for determining of schisandrin in Weiganfutai capsule （ginseng stem-leaf saponin, extractive material from Fructus Schisandrae Chinese, Ganoderm applanatum polysaccharide, etc. ）. Methods A YMC C18 column was used. The mobile phase was a mixed liquid with methanol-0. 03% phosphoricalid（65 ： 35 ） , and determination wavelength was 250 nm. Results The linear ranges of schisandrin was 0. 142 - 1. 140 μg （ r = 0. 999 7 ）, respectively. The average recoveries of schisandrin was 99.49% （ RSD = 1.93% ）, respectively. Conclusions The method is simple, accurate, and can be used for the quality control of Weiganfutai capsule. |
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| Keywords: | RP-HPLC Weiganfutai capsule Schisandrin Determination |
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