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染色黄柏中金胺O的检测方法研究
引用本文:吴萌,饶伟文.染色黄柏中金胺O的检测方法研究[J].中国药师,2011,14(8):1112-1114.
作者姓名:吴萌  饶伟文
作者单位:桂林食品药品检验所 广西桂林541002
基金项目:科技部国家重大新药创制-创新药物研究开发技术平台建设课题
摘    要:目的:对市售黄柏染色品中化工染料进行鉴定,并研究其定量检测方法。方法:采用TLC法、HPLC-PAD法、HPLC-MS法,对多批市售黄柏样品进行定性、定量分析。结果:经检测8批市售品,有7批检出金胺O,其含量在20~110mg/100 g。结论:黄柏染色用化工染料为金胺O,本文建立的检测方法,可满足定性定量检测的要求。

关 键 词:黄柏  金胺O  TLC法  HPLC-MS法

Study on the Determination Methods for Auramine O in Phellodendri Chinensis Cortex
Wu Meng,Rao Weiwen.Study on the Determination Methods for Auramine O in Phellodendri Chinensis Cortex[J].China Pharmacist,2011,14(8):1112-1114.
Authors:Wu Meng  Rao Weiwen
Institution:Wu Meng,Rao Weiwen(Guilin Institute for Food and Drug Control,Guangxi Guilin 541002,China)
Abstract:Objective:To identify the chemical dye in Phellodendri Chinensis Cortex,and study its determination method.Method: The dye was identified by TLC,HPLC-PAD and HPLC-MS.The dye content in Phellodendri Chinensis Cortex was determined by HPLC. Result:Among eight batches of Phellodendri Chinensis Cortex,auramine O was detected in seven batches with the content range of 20 to 110 mg/100 g.Conclusion:The chemical dye in Phellodendri Chinensis Cortex is auramine O.The method can meet the requirements of identificati...
Keywords:Phellodendri Chinensis Cortex  Auramine O  TLC  HPLC-MS  
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