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二阶导数光谱法测定七厘散中血竭的含量
引用本文:席琳图雅,布和巴特. 二阶导数光谱法测定七厘散中血竭的含量[J]. 北方药学, 2011, 8(7): 6-7
作者姓名:席琳图雅  布和巴特
作者单位:内蒙古民族大学蒙医药学院,通辽,028000;内蒙古民族大学蒙医药学院,通辽,028000
摘    要:目的:用二阶导数光谱法测定七厘散中血竭的含量。方法:采用二阶导数光谱法,峰-峰法量取264-262nm附近峰谷间极距P来测定七厘散中血竭的含量。结果:血竭线性范围0.024~0.072mg/ml,r=0.9999,平均回收率101.2%,CV为4.7%。结论:以此法控制七厘散的内在质量,不经分离提纯,即可消除其他药的干扰。

关 键 词:七厘散  血竭  二阶导数光谱

Determination of the content of Resina Draconis in Qili Powder by second order derivative spectrophotometry method
Xinlintuya,Buhebate. Determination of the content of Resina Draconis in Qili Powder by second order derivative spectrophotometry method[J]. BEIFANG YAOXUE, 2011, 8(7): 6-7
Authors:Xinlintuya  Buhebate
Affiliation:Xinlintuya Buhebate(College of Mongolian Medicine and Pharmacy,Inner Mongolia University for the Nationalities,Tongliao 028000 China)
Abstract:Objective:To establish a second order derivative spectrophotometry method for determination of the content of Resina Draconis in Qili Powder.Methods:The second order derivative spectrophotometry method was performed at the wavelength of 264-262nm.Result:Resina Draconis showed a good linear relationship within a range of 0.024-0.072mg/ml,r=0.9999.The average recovery rate was 101.2%,CV=4.7.Conclusion:The method for determination of the content of Resina Draconis in Qili Powder is simple and accurate.The method could eliminate the interference from other medicinal herbs,so the compound herbs don't need to be purified.
Keywords:Qili Powder Resina Draconis Second order derivative spectrophotometry method
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