| 祛风活络酒质量标准研究 |
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| 引用本文： | 吕建伟,吴红文.祛风活络酒质量标准研究[J].海峡药学,2009,21(8):62-63. |
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| 作者姓名： | 吕建伟 吴红文 |
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| 作者单位： | 1. 广西柳州市中医院,柳州,545001
2. 广西柳州市工人医院,柳州,545005 |
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| 摘 要： | 目的建立祛风活络酒的质量标准。方法采用TLC法对处方中续断、茜草进行定性鉴别；用HPLC法测定祛风活络酒中阿魏酸的含量。结果TLC色谱特征明显，阴性无干扰，专属性强；阿魏酸在1．9～60．8μg·mL^-1浓度范围内线性关系良好，r=0．9999，平均加样回收率为100．10％．RSD为2．2％（n=6）。结论所建标准可用于祛风活络酒的质量控制。
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| 关 键 词： | 祛风活络酒 阿魏酸 高效液相色谱法 薄层色谱法 质量标准 |
Quality standard of Qufen Huoluo Vinum |
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| LU Jian-wei,WU Hong-wen.Quality standard of Qufen Huoluo Vinum[J].Strait Pharmaceutical Journal,2009,21(8):62-63. |
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| Authors: | LU Jian-wei WU Hong-wen |
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| Institution: | LU Jian-wei, WU Hong-wen (1 .Liuzhou Traditional Chinese Medicine Hospital, Liuzhou 545001, China; 2. Liuzhou worker＇s Hospital, Liuzhou 545005, China) |
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| Abstract: | OBJECTIVE To establish the quality standard of Qufen Huoluo Vinum. METHODS Radix dipsaci and Radix et rhizoma rubiae were identified by TLC; and the contents of ferulic acid in Qufen Huoluo Vinum were determinded by HPLC. RESULTS The TLC characteristics were distinctive and specific, and there was no interference in negative control. The linear concentration of ferulic acid was 1.9 - 60.8μg· mL^- 1 （r = 0. 9999） and the average recovery was 100.10 %, RSD 2.2 % .CONCLUSION The established sfandard can be used for the quality control of Qufen Huoluo Vinum. |
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| Keywords: | Qufen Huoluo Vinum Ferulic acid HPLC TLC Quality standard |
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