| 槟榔花中槟榔碱的热回流提取工艺优化 |
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| 引用本文： | 战晴晴,周亚奎,卢丽兰,刘洋洋,甘炳春.槟榔花中槟榔碱的热回流提取工艺优化[J].中国实验方剂学杂志,2013,19(14):77-79. |
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| 作者姓名： | 战晴晴 周亚奎 卢丽兰 刘洋洋 甘炳春 |
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| 作者单位： | 中国医学科学院北京协和医学院药用植物研究所海南分所,海南省南药资源保护与开发重点实验室,海南万宁571533 |
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| 基金项目： | 海南省中药现代化专项(2011ZY008);海南省自然科学基金项目(311094,310109);"十二五"国家科技支撑计划项目 (2011BAI01B07) |
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| 摘 要： | 目的:研究槟榔花中槟榔碱的热回流提取最佳工艺.方法:以氢溴酸槟榔碱提取含量为考察指标,采用L9(34)正交试验研究料液比、提取时间和提取次数3个因素对槟榔花中热回流提取槟榔碱的影响,得出槟榔花中槟榔碱的最佳提取工艺.结果:从槟榔花中热回流提取槟榔碱的最佳工艺为料液比1∶80,提取时间25 min,提取次数3次.最佳条件下槟榔碱提取含量可达(4.31 ±0.047) mg·g-1.结论:该工艺简单、高效,能有效提取槟榔花中的槟榔碱,与旧工艺的提取含量(3.38±0.03) mg·g-1有显著性差异.
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| 关 键 词： | 槟榔花 氢溴酸槟榔碱 热回流 高效液相色谱 |
| 收稿时间： | 2012/10/12 0:00:00 |
Optimization of Heat Reflux Extraction of Arecoline from Areca inflorescence |
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| ZHAN Qing-qing,ZHOU Ya-kui,LU Li-lan,LIU Yang-yang and GAN Bing-chun.Optimization of Heat Reflux Extraction of Arecoline from Areca inflorescence[J].China Journal of Experimental Traditional Medical Formulae,2013,19(14):77-79. |
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| Authors: | ZHAN Qing-qing ZHOU Ya-kui LU Li-lan LIU Yang-yang and GAN Bing-chun |
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| Institution: | Hainan Branch Institute of Medicinal Plant, Chinese Academy of Medical Sciences & Peking Union Medical College, Hainan Provincial Key Laboratory of Resource Conservation and Development of Southern Medicine, Wanning 571533, China;Hainan Branch Institute of Medicinal Plant, Chinese Academy of Medical Sciences & Peking Union Medical College, Hainan Provincial Key Laboratory of Resource Conservation and Development of Southern Medicine, Wanning 571533, China;Hainan Branch Institute of Medicinal Plant, Chinese Academy of Medical Sciences & Peking Union Medical College, Hainan Provincial Key Laboratory of Resource Conservation and Development of Southern Medicine, Wanning 571533, China;Hainan Branch Institute of Medicinal Plant, Chinese Academy of Medical Sciences & Peking Union Medical College, Hainan Provincial Key Laboratory of Resource Conservation and Development of Southern Medicine, Wanning 571533, China;Hainan Branch Institute of Medicinal Plant, Chinese Academy of Medical Sciences & Peking Union Medical College, Hainan Provincial Key Laboratory of Resource Conservation and Development of Southern Medicine, Wanning 571533, China |
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| Abstract: | Objective: To study the condition of heat reflux extraction of arecoline from Areca inflorescence. Method: With yield of arecoline as index, effect of solid-liquid ratio, extraction time and extraction times on the yield of arecoline was investigated by L9 (34) orthogonal test to obtain the best extraction conditions. Result: The optimum condition of heat reflux extraction of arecoline from A. inflorescence was as follows:ratio of liquid to material 80:1, extraction time 25 min, 3 times for extraction. The yield of arecoline was (4.31±0.047) mg·g-1. Conclusion: This optimized technology is simple, efficient and suitable for extraction of arecoline from A. inflorescence. It has significant differences compared with old heat reflux extraction technology which yield of arecoline is (3.38±0.03) mg·g-1. |
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| Keywords: | Areca inflorescence arecoline heat reflux extraction HPLC |
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