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飞龙掌血挥发性化学成分的GC-MS分析
引用本文:刘志刚,李莹,朱芳芳,何娅,袁淼淼,徐明江.飞龙掌血挥发性化学成分的GC-MS分析[J].辽宁中医学院学报,2011(11):150-151.
作者姓名:刘志刚  李莹  朱芳芳  何娅  袁淼淼  徐明江
作者单位:贵阳学院生物与环境工程系,贵州贵阳550003
基金项目:贵阳学院20l0年学生科研项目课题(201002)
摘    要:目的:研究民族药飞龙掌血中挥发性化学成分。方法:采用水蒸气蒸馏的方法提取飞龙掌血中挥发油成分,通过正交设计法优选了提取飞龙掌血挥发油的工艺条件;采用气相色谱-质谱联用法(GC-MS)对飞龙掌血挥发油中的化学成分进行了分离鉴定。结果:最佳提取条件为药材粉碎40目,用10倍量水浸泡过夜,连续提取12h,在最佳工艺条件下,飞龙掌血挥发油得率为0.12%,经GC-MS分析,从飞龙掌血挥发油中共鉴定出26个化学成分,鉴定率为97.4%,其主要化学成分为α-杜松醇、斯巴醇、α-紫穗槐烯等。结论:飞龙掌血根和叶挥发油成分差异较大。

关 键 词:飞龙掌血  挥发油  GC-MS

Study on Chemical Composition of the Essential Oil from Toddalia Asiatica Lain. by Gas Chromatography/Mass Spectrum
LIU Zhi-gang,LI Ying,ZHU Fang-fang,HE Ya,YUAN Miao-miao,XU Ming-jiang.Study on Chemical Composition of the Essential Oil from Toddalia Asiatica Lain. by Gas Chromatography/Mass Spectrum[J].Journal of Liaoning College of Traditional Chinese Medicine,2011(11):150-151.
Authors:LIU Zhi-gang  LI Ying  ZHU Fang-fang  HE Ya  YUAN Miao-miao  XU Ming-jiang
Institution:(Department of Biology and Environment Engineering,Guiyang College,Guiyang 550003,Guizhou,China)
Abstract:Objective:To study the chemical compositions of essential oil from Toddalia asiatica Lam..Methods:The essential oil from Toddalia asiatica Lam.was prepared by the method of Steam Distillation and its chemical compositions were analyzed by GC/MS.Results:The optimal conditions were determined by orthogonal test as follows:40 mesh of samples,12h of extraction time,and 10 times of extraction solvent.Under the optimal conditions,the oil yield was 0.12%.26 compounds were identified,in which the main ingredients were α-Cadinol,spathulenol and α-Amorphene,etc.Conclusion:The chemical compositions of the bark are different from the leaves in the essential oil of Toddalia asiatica Lam.
Keywords:Toddalia asiatica Larn    essential oil  GC-MS
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