| RP-HPLC法测定健肝灵胶囊中五味子醇甲的含量 |
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| 引用本文： | 孙强,何召允,王传杰,靳维荣. RP-HPLC法测定健肝灵胶囊中五味子醇甲的含量[J]. 辽宁中医学院学报, 2010, 0(11): 224-225 |
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| 作者姓名： | 孙强 何召允 王传杰 靳维荣 |
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| 作者单位： | [1]山东省泰安市药品检验所,山东泰安271000 [2]山东省泰安市食品药品监督管理局,山东泰安271000 [3]泰安市中心医院,山东泰安271000 [4]山东省农业科学院农产品研究所,山东济南250100 |
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| 摘 要： | 目的：建立反相高效液相色谱法（RP-HPLC法）测定健肝灵胶囊中五味子醇甲的含量。方法：采用Shimadzu C18（250mm×4.6mm,5μm）色谱柱,甲醇-水（65∶35）为流动相;流速为1.0mL.min-1;柱温为40℃;检测波长为250nm。结果：五味子醇甲在0.426-2.13μg范围内呈现良好的线性关系,相关系数r=0.9999;平均回收率为99.71%,RSD为1.07%（n=5）。结论：所建立的RP-HPLC含量测定方法准确、快速,专属性强,重现性好。
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| 关 键 词： | 反相高效液相色谱法 五味子醇甲 健肝灵胶囊 含量测定 |
RP-HPLC Determination of Schisandrin in Jianganling Capsules |
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| RP-HPLC Determination of Schisandrin in Jianganling CapsulesSUN Qiang,HE Zhao-yun,WANG Chuan-jie,JIN Wei-rong. RP-HPLC Determination of Schisandrin in Jianganling Capsules[J]. Journal of Liaoning College of Traditional Chinese Medicine, 2010, 0(11): 224-225 |
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| Authors: | RP-HPLC Determination of Schisandrin in Jianganling CapsulesSUN Qiang HE Zhao-yun WANG Chuan-jie JIN Wei-rong |
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| Affiliation: | 1.Taian City Institute of Drug Control,Tai＇an 271000,Shandong,China;2.Taian City Food and Drug Administration,Tai＇an 271000,Shandong,China;3.The Central Hospital of Taian,Tai＇an 271000,Shandong,China;4.Institute of Agro-Food Science and Technology,Shandong Academy of Agricultural Sciences,Ji＇nan 250100,Shandong,China) |
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| Abstract: | Objective：An RP-HPLC method was established for the determination of Schisandrin in Jianganling Capsules.Methods：Using Shimadzu column C18（250mm×4.6mm,5μm）,the mobile phase was a mixture of methanol-water（65∶35）at a flow rate of 1.0 mL.min-1.The column temperature was 40 ℃,and the UV detection was set at 250nm.Results：The calibration curve was liner in the range of 0.426~2.13μg（r=0.9999）,the recovery rate was 99.71% and the RSD was 1.07%（n=5）.Conclusion：The method is accurate,simple and reproducible for the assay of.Schisandrin. |
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| Keywords: | RP-HPLC schisandrin Jianganling capsules assay |
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