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泽泻药材与饮片的质量标准研究
引用本文:徐浩坤,胡浩彬,郑云枫,彭国平,张同星,李存玉. 泽泻药材与饮片的质量标准研究[J]. 辽宁中医学院学报, 2010, 0(11): 26-27
作者姓名:徐浩坤  胡浩彬  郑云枫  彭国平  张同星  李存玉
作者单位:[1]南京中医药大学,江苏南京210029 [2]江苏省药品检验所,江苏南京210008
基金项目:国家药典委员会资助项目(YZ-126YZ-127)
摘    要:目的:研究泽泻药材与饮片的质量标准。方法:对泽泻药材与饮片进行性状鉴别、显微鉴别、薄层鉴别,并用高效液相法测定其中23-乙酰泽泻醇B的含量。结果:总结了泽泻药材与饮片的主要鉴别特征;23-乙酰泽泻醇B浓度在0.925-59.2μg/mL范围内与峰面积积分值呈良好的线性关系(r=0.9999);平均回收率为103.24%,RSD=1.53%(n=6)。结论:所建标准可用于泽泻药材与饮片的质量控制。

关 键 词:泽泻  饮片  质量标准  23-乙酰泽泻醇B

Study on Quality Standard of Alismatis Orientalis and Alismatis Slices
XU Hao-kun,HU Hao-bin,ZHENG Yun-feng,PENG Guo-ping,ZHANG Tong-xing,LI Cun-yu. Study on Quality Standard of Alismatis Orientalis and Alismatis Slices[J]. Journal of Liaoning College of Traditional Chinese Medicine, 2010, 0(11): 26-27
Authors:XU Hao-kun  HU Hao-bin  ZHENG Yun-feng  PENG Guo-ping  ZHANG Tong-xing  LI Cun-yu
Affiliation:1.Nanjing University of Chinese Medicine,Nanjing 210029,Jiangsu,China;2.Jiangsu Institute of Drug Inspection,Nanjing 210008,Jiangsu,China)
Abstract:Objective:To study the quality standard of Alismatis orientalis and Alismatis slices.Methods:The characteristic study,microscopic identification and TLC identification of Alismatis slices were performed,and the content of alisol B 23-acetate in which was determined by HPLC.Results:The chief characteristics of Alismatis orientalis and Alismatis slices have been summarized.The linear range of alisol B 23-acetate was 0.925~59.2μg/mL(r = 0.9999)with its average recovery at 103.24%(RSD=1.53%,n=6).Conclusion:The established standard can be used for the quality control of Alismatis orientalis and Alismatis slices.
Keywords:Alismatis orientalis(Sam.)  Pieces  quality standards  alisol B 23-acetate
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