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| 解肌宁嗽丸中葛根素含量的测定研究 | |
| 引用本文： | 曲静,刘丽,尹程鑫. 解肌宁嗽丸中葛根素含量的测定研究[J]. 实用中医内科杂志, 2011, 25(4): 32-33. DOI: 10.3969/j.issn.1671-7813.2011.04.15 |
| 作者姓名： | 曲静 刘丽 尹程鑫 |
| 作者单位： | 1. 辽宁中医药大学,辽宁沈阳,110032 2. 辽宁成大生物股份有限公司,辽宁沈阳,110026 |
| 摘 要： | [目的]建立解肌宁嗽丸的质量控制方法。[方法]建立HPLC法测定制剂中葛根素含量的方法。色谱柱:C18(250×4.6mm,5μm),柱温:25℃;流动相:甲醇-水(25:75),流速:1.0mL·min-1,检测波长:250nm。[结果]葛根素在0.338～1.690μg范围内线性关系良好,R=0.9999。[结论]本方法简便、准确,重复性好,可作为解肌宁嗽丸的质量控制方法。 |
| 关 键 词： | 解肌宁嗽丸 葛根素 HPLC法 |
Determination of Puerarin Contents in Jiejiningsou Pills |
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| QU Jing,LIU Li,YIN Cheng-xin. Determination of Puerarin Contents in Jiejiningsou Pills[J]. , 2011, 25(4): 32-33. DOI: 10.3969/j.issn.1671-7813.2011.04.15 | |
| Authors: | QU Jing LIU Li YIN Cheng-xin |
| Affiliation: | 1.Liaoning University of Traditional Chinese Medicine,Shenyang 110032,Liaoning,China; 2.Liaoning Chengda Biotechnology Co.Ltd,Shenyang 110026,Liaoning,China) |
| Abstract: | [Objective]To establish a HPLC method for determination Puerarin in Jiejiningsou Pills.[Method]The column was C18(250×4.6mm,5μm).The mobile phase was methanol-water(25:75)and the flowrate was 1.0mL·min-1.The detection wavelength was at 250nm.[Results]Puerarin has a good linear between 0.338-1.690μg.[Conclusion]The method is smiple and accurate with good repeatability and can be used for the quality control of Puerarin in Jiejiningsou Pills. |
| Keywords: | Jiejiningsou Pills Puerarin HPLC |
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