| 多指标正交试验优选双花解毒颗粒中水提部分提取工艺 |
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| 引用本文： | 丁志军,廖银根,罗美兰,谭志江.多指标正交试验优选双花解毒颗粒中水提部分提取工艺[J].江西中医学院学报,2012,24(1):45-47. |
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| 作者姓名： | 丁志军 廖银根 罗美兰 谭志江 |
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| 作者单位： | 江西省皮肤病专科医院,南昌,330001 |
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| 摘 要： | 目的：优选双花解毒颗粒水提部分提取工艺。方法：采用正交试验设计,以绿原酸、芍药苷含量及干膏率为指标,选取L9（34）正交表,优化提取工艺中加水量、煎煮次数、煎煮时间3个因素。结果：以饮片投料,加12倍量的水煎煮2次,第一次1.5h,第二次1.0 h为最佳工艺。结论：该工艺稳定可靠,可用于生产。
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| 关 键 词： | 双花解毒颗粒 正交试验 综合评分法 高效液相色谱法 |
Optimization of Extraction Technology of the Water Extraction Part in Shuanghua Detoxification Granules by Orthogonal Design with Multi-targets |
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| DING Zhi-jun
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LIAO Yin-gen
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LUO Mei-lan
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TAN Zhi-jiang.Optimization of Extraction Technology of the Water Extraction Part in Shuanghua Detoxification Granules by Orthogonal Design with Multi-targets[J].Journal of Jiangxi College of Traditional Chinese Medicine,2012,24(1):45-47. |
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| Authors: | DING Zhi-jun LIAO Yin-gen LUO Mei-lan TAN Zhi-jiang |
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| Institution: | Jiangxi Specialized subject hospital of skin,Nanchang 330001,China |
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| Abstract: | Objective:To optimize the extraction technology for the water extraction part in Shuanghua detoxification Granules.Methods:With the yield of extracts yield and the contents of Chlorogenic acid and Paeoniflorin as indexes,orthogonal table L9(34)was used in the experiment of extracting in water to study the effect of technological parameters(the dosage of water,extraction times,the time of extraction)on the content of Chlorogenic acid and Paeoniflorin.Results:The optimum process is that water is used as extracting solution adding 12 times amount of solution,extracting 2 times,1.5 hours for the first time and 1.0 hour for the second time.Conclusion:The extraction process is stable and suitable for industrial production. |
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| Keywords: | Shuanghua detoxification Orthogonal test Grading methods HPLC |
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