| 不同栽培类型菊花挥发性成分的固相微萃取-气相色谱-质谱分析 |
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| 引用本文： | 周海梅,谢培山,李朴,马锦琦,吴云骥. 不同栽培类型菊花挥发性成分的固相微萃取-气相色谱-质谱分析[J]. 解放军药学学报, 2008, 24(1): 33-36 |
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| 作者姓名： | 周海梅 谢培山 李朴 马锦琦 吴云骥 |
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| 作者单位： | 河南科技大学法医学院,河南,洛阳,471003;珠海科曼中药研究有限公司,广东,珠海,519000 |
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| 基金项目： | 致谢!洛阳市陆生天然植物研究所王忠东所长提供菊花样品并予以鉴定,在此表示衷心感谢. |
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| 摘 要： | 目的分析不同栽培类型菊花的挥发性成分。方法用顶空固相微萃取（HS—SPME）结合气相色谱-质谱联用技术（GC—MS）对菊花的挥发性成分进行鉴定，用面积归一法测定其相对含量。结果鉴定出11种菊花的挥发性成分共83个。结论SPME技术操作简便，能准确反映菊花的挥发性组分；11个类型菊花的挥发性成分和含量有显著差异。
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| 关 键 词： | 固相微萃取 GC-MS 菊花 挥发性成分 |
| 文章编号： | 1008-9926(2008)01-0033-04 |
| 修稿时间： | 2006-12-28 |
Analysis of Volatile Components of Various Chrysanthemum Morifolium by SPME GC-MS |
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| ZHOU Hai-Mei,XIE Pei-Shan,LI Pu,MA Jin-Qi,WU Yun-Ji. Analysis of Volatile Components of Various Chrysanthemum Morifolium by SPME GC-MS[J]. Pharmaceutical Journal of Chinese People's Liberation Army, 2008, 24(1): 33-36 |
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| Authors: | ZHOU Hai-Mei XIE Pei-Shan LI Pu MA Jin-Qi WU Yun-Ji |
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| Affiliation: | ZHOU Hai-Mei, XIE Pei-Shan, LI Pu, MA Jin-Qi ,WU Yun-Ji (1 Faculty of Forensic Medicine, Henan University of Science and Technology, Luoyang 471003, Henan China;2 Zhuhai ChroMap Institute of Herbal Medicine Research, Zhuhai 519000, Guangdong China) |
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| Abstract: | Aim To analyze volatile components from various Chrysanthemum Morifolium Ramat. Methods The volatile components were separated and identified by head space solid-phase microextraction （HS-SPME） and gas chromatography-mass spectrometry （ GC-MS）, and their relative contents were determined by normalization of the area. Results 83 compounds from eleven kinds of Chrysanthemum Morifolium Ramat were identified by SPME-GC- MS. Conclusion SPME is simple and user-friendly, and can report accurately volatile components of Chrysanthemum Morifolium Ramat. There are significant differences in the volatile composition and content of eleven kinds of Chrysanthemum Morifolium Ramat. |
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| Keywords: | Solid-phase microextraction （ SPME ） Gas chromatography-mass spectrometry （ GC-MS ） Chrysanthemum Morifolium Ramat. Volatile component |
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