砷酸基苯乙酮类化合物的高效简便合成

目的合成砷酸基苯乙酮类化合物及研究高效、环境保护的合成方法，奠定研究砷制剂苯乙酮类化合物的构效关系基础。方法利用微波加热研究了微波输出功率，辐射时间以及不同溶剂对反应速度及收率的影响，同时与常规加热反应做对比。结果合成了砷酸基苯乙酮类化合物。结论此法操作简便，收率较高，副产物少，为进一步研究微波技术在有机合成中的应用以及砷制剂苯乙酮类化合物的制备具有一定价值。

Convenient and efficient synthesis of arsonic acid-acetophenone

Objective A series of arsonie aeid-aeetophenone were synthesized under microwave irradiation and to study the Synthetic method of high performance and environmental protection. Methods The effects of microwave power, irradiation time and different solvents on the reaction were dicussed, in addition, compared with the conventional heating reaction. Results The structures of the compound were authenticated . Conclusions The results show that microwave thechnology is a method of simplity, security, rapidity with a high yield.