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| HPLC法测定复方益肝丸中丹皮酚的含量 | |
| 引用本文： | 章贵杰,刘丽,赵春香. HPLC法测定复方益肝丸中丹皮酚的含量[J]. 中国药师, 2009, 12(1): 91-92 |
| 作者姓名： | 章贵杰 刘丽 赵春香 |
| 作者单位： | 1. 吉林省人民医院,吉林长春,130021 2. 吉林省四平市食品药品检验所 3. 吉林省食品药品检验所 |
| 摘 要： | 建立复方益肝丸中丹皮酚的HPLC测定方法。方法：采用SHISEIDO CAPCELL PAKC18色谱柱（250mm×4．6mm，5μm），乙腈-水（38：62）为流动相；检测波长为274nm。结果：丹皮酚线性范围为0．043～0．869μg，平均加样回收率为99．8％，RSD=0．8％（n=6）。结论：该方法重复性好，结果准确，可用于该制剂的质量控制。 |
| 关 键 词： | HPLC 复方益肝丸 丹皮酚 |
Determination of Paeonol in Compound Yigan Pills by HPLC |
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| Zhang Guijie,Liu Li,Zhao Chunxiang. Determination of Paeonol in Compound Yigan Pills by HPLC[J]. China Pharmacist, 2009, 12(1): 91-92 | |
| Authors: | Zhang Guijie Liu Li Zhao Chunxiang |
| Affiliation: | Zhang Guijie (Jilin Provincial People＇s Hospital, Jilin, Changchun 130021, China) ; Liu Li( Siping Instiuite for Food and Drug Control, Jilin) ; Zhao Chunxiang (Jilin Provincial Institute for Food and Drug Control) |
| Abstract: | To establish the method to determine the content of paeonol in compound Yigan pills by HPLC. Method： The determination was carried out on SHISEIDO CAPCELL PAKC18 column（ 250mm × 4.6mm ,5 μm） with mobile phase of acetonitrilewater（38： 62） and detection wavelength at 274nm. Result： The linear range was 0. 043 to 0. 869μg for paeonol. The average recovery was 99.8% , and RSD was 0.8% （n = 6 ）. Conclusion： The method is accurate and highly reproducible. It can be a method for quality control of compound Yigan pills. |
| Keywords: | HPLC |
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