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山芝麻挥发油成分的GC-MS分析
引用本文:苏丹,高玉桥,黄增芳,梅全喜. 山芝麻挥发油成分的GC-MS分析[J]. 中国药房, 2011, 0(23): 2173-2174
作者姓名:苏丹  高玉桥  黄增芳  梅全喜
作者单位:电子科技大学中山学院;广州中医药大学附属中山医院;
基金项目:中山市科技计划项目(医疗卫生)(20102A108)
摘    要:
目的:用气相色谱-质谱(GC-MS)联用法对山芝麻挥发油进行化学成分的分析。方法:采用水蒸气蒸馏法从山芝麻中提取挥发油,用GC-MS联用法对化学成分进行鉴定,采用峰面积归一法测定其含量。结果:共鉴定了81个成分,占挥发油总成分的76.52%;主要为单萜烯类、倍半萜烯类及其含氧衍生物和脂肪族化合物等。结论:本方法稳定、可靠,重现性好,适用于中药挥发油的化学成分分析。

关 键 词:山芝麻  挥发油  气相色谱-质谱联用法

Analysis of Volatile Oil in Helicteres angustifolia by GC-MS
SU Dan,HUANG Zeng-fang GAO Yu-qiao,MEI Quan-xi. Analysis of Volatile Oil in Helicteres angustifolia by GC-MS[J]. China Pharmacy, 2011, 0(23): 2173-2174
Authors:SU Dan  HUANG Zeng-fang GAO Yu-qiao  MEI Quan-xi
Affiliation:SU Dan,HUANG Zeng-fang(Zhongshan College,University of Electronic Science and Technology of China,Zhongshan 528400,China) GAO Yu-qiao,MEI Quan-xi(Zhongshan Hospital,Guangzhou University of TCM,China)
Abstract:
OBJECTIVE:To analyze the chemical components of volatile oil from Helicteres angustifolia by GC-MS.METHODS:The volatile oil was extracted from H.angustifolia by steam distillation.The chemical components of volatile oil were identified by GC-MS,the content of chemical components from volatile oil were determined by normalization method.RESULTS:There were 81 chemical components,accounting for 76.52% of total volatile oil.Main chemical components were monoterpenes,sesquiterpenes and their oxygenated derivativ...
Keywords:Helicteres angustifolia  Volatile oil  GC-MS  
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