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| 消瘤胶囊的质量标准研究 | |
| 引用本文： | 顾和亚,周琴妹,梁海宁,李悦予,刘汉清. 消瘤胶囊的质量标准研究[J]. 现代中药研究与实践, 2012, 0(1): 70-73 |
| 作者姓名： | 顾和亚 周琴妹 梁海宁 李悦予 刘汉清 |
| 作者单位： | 江苏省中医院;甘肃省中医院;南京中医药大学 |
| 摘 要： | 目的建立消瘤胶囊的质量标准。方法采用薄层色谱法鉴别处方药材党参、丹参、三棱。采用高效液相色谱测定制剂中的斑蝥素含量。结果薄层色谱鉴别在与对照药材相应的位置上,分别显相同颜色的斑点,方法专属性强,阴性对照无干扰。含量测定,斑蝥素的回归方程为:A=630.556 9C-8.628 57,r=0.999 9。浓度在0.097 25~0.778 mg/mL范围内线性关系良好。消瘤胶囊中斑蝥素含量拟控制在1.5%以上。结论本方法简便、准确、重现性好,可用于消瘤胶囊的质量控制。 |
| 关 键 词： | 消瘤胶囊 质量标准 薄层色谱法 高效液相色谱法 |
Study on Quality Standard for Xiaoliu Capsule |
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| GU He-ya,ZHOU Qin-mei,LIANG Hai-nin,LI Yue-yu,LIU Han-qing. Study on Quality Standard for Xiaoliu Capsule[J]. Research and Practice on Chinese Medicines, 2012, 0(1): 70-73 | |
| Authors: | GU He-ya ZHOU Qin-mei LIANG Hai-nin LI Yue-yu LIU Han-qing |
| Affiliation: | 1.Jiangsu Provincial Hospital of Traditional Chinese Medicine,Nanjing 210029,China;2.Gansu Provincial Hospital of Traditional Chinese Medicine,Lanzhou 730050,China;3.Nanjing University of TCM,Nanjing 210029,China) |
| Abstract: | Objective To establish the quality standard for Xiaoliu Capsule.Methods Codonopsis Radix,Salviae miltiorahizae Radix et Rhizoma and Sparganii Rhizoma Tuber were identified by TLC;HPLC method was used to determine the content of cantharidin.Results The TLC spots were quite clear;The calibration curve of cantharidin was linear within the range of 0.097 25～0.778 mg/mL,and the regression equation was A=630.556 9C-8.628 57,(r=0.999 9).Conclusion The method was simple,accurate and reproducible,and could be used for the quality control of Xiaoliu Capsule. |
| Keywords: | Xiaoliu Capsule quality standard TLC HPLC |
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