| HPLC法测定清开灵注射液中黄芩苷的含量 |
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| 引用本文： | 庞树和,李莉,张久华. HPLC法测定清开灵注射液中黄芩苷的含量[J]. 中国药品标准, 2004, 5(3): 58-60 |
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| 作者姓名： | 庞树和 李莉 张久华 |
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| 作者单位： | 1. 黑龙江省绥化市药品检验所,绥化,152062
2. 哈药集团三精制药绥化有限公司,152061 |
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| 摘 要： | 目的:测定清开灵注射液中黄芩苷的含量.方法:采用高效液相色谱法,十八烷基硅烷键合硅胶填充剂,流动相为甲醇:水:冰醋酸,检测波长为274nm,结果平均加样回收率为100.2%;结论:方法简便,快速,灵敏度高,可用于清开灵注射液中黄芩苷的含量控制.
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| 关 键 词： | 高效液相色谱法 黄芩苷 含量测定 |
Determination of the Content of Baicalin in Qing Kai Ling Injection by HPLC |
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| Pang Shuhe,Li Li and Zhang Jiuhua. Determination of the Content of Baicalin in Qing Kai Ling Injection by HPLC[J]. , 2004, 5(3): 58-60 |
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| Authors: | Pang Shuhe Li Li Zhang Jiuhua |
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| Affiliation: | Heilongjiang Provincial Suihua Institute of Drug Control, Suihua 152062;Heilongjiang Provincial Suihua Institute of Drug Control, Suihua 152062;Suihua Corporation Haerbin Pharmaceutical Group |
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| Abstract: | Objective:To establish a method of quantitative analysis of baicalin in qing kai ling injection. Method:To determine the Content of baicalin in qing kai ling injection by HPLC, using a column packed with C18 and a mixture of methanol-water-glacial acetic acid as the mobile phase,detection wavelength is 274nm. Result: The mean recoveries of baicalin were 100. 2%. Conclusion: The method is simple,accurate and reliable. |
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| Keywords: | Baicalin Assay HPLC |
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