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| 应用均匀设计研究2-甲基-5-巯基-1,3,4-噻二唑制备工艺 | |
| 引用本文： | 王旭,李敬芬,周淑晶,周天明. 应用均匀设计研究2-甲基-5-巯基-1,3,4-噻二唑制备工艺[J]. 中国现代应用药学, 1998, 15(2): 31-32 |
| 作者姓名： | 王旭 李敬芬 周淑晶 周天明 |
| 摘 要： | 应用均匀于标题化合物工艺研究中，以乙酸乙酸和水合肼于二甲苯中反应，加入ＣＳ２，直接加热，一步环合成标题化合物，总收率达７５．５％。 |
| 关 键 词： | 均匀设计 噻二唑 制备 头孢唑啉 |
Investigation of preparation of 2-Methyl-5-Mercapto-1 ,3,4-Thiadiazole with uniform design |
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| Wang Xu (Wang X,Li Jingfen (Li JF ,Zhou Shujing (Zhou SJ,et al. Investigation of preparation of 2-Methyl-5-Mercapto-1 ,3,4-Thiadiazole with uniform design[J]. The Chinese Journal of Modern Applied Pharmacy, 1998, 15(2): 31-32 | |
| Authors: | Wang Xu (Wang X Li Jingfen (Li JF Zhou Shujing (Zhou SJ et al |
| Abstract: | The uniform design was applied to technological study of the title compound, starting from ethyl acetate and diamine hydrate,followed by reaction with carbon disulfide,the title compound was synthesized in one step.The overall yield amounts to 75.5% . |
| Keywords: | uniform desing 2-methyl-5-mercapto-1 3 4-thiadiazole praparation |
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