| 植物生长调节剂DA-6的合成研究 |
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| 引用本文： | 汤昆,邱金东.植物生长调节剂DA-6的合成研究[J].河南大学学报(医学版),2006,25(2):26-27. |
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| 作者姓名： | 汤昆 邱金东 |
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| 作者单位： | 1. 河南大学医学院,有机教研室,河南,开封,475001
2. 河南大学,药学院,河南,开封,475001 |
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| 摘 要： | 目的:采用改性硫酸钛作催化剂合成DA-6。方法:通过正交试验确定了合成的最佳工艺条件。结果:醇酸摩尔比1.1∶1,反应时间10h,催化剂用量0.033mol/mol己酸,产品酯化率可达95%以上。结论:此优化条件合理可行,为工业生产提供了科学依据。
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| 关 键 词： | 改性硫酸钛 植物生长调节剂(DA-6) 酯化 |
| 文章编号： | 1672-7606(2006)02-0026-02 |
| 收稿时间： | 2006-03-23 |
| 修稿时间： | 2006年3月23日 |
Synthesis of (DA -6) Plant Growth Hormone |
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| TANG Kun,QIU Jin-dong.Synthesis of (DA -6) Plant Growth Hormone[J].Journal of Henan University,2006,25(2):26-27. |
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| Authors: | TANG Kun QIU Jin-dong |
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| Institution: | 1. Medical college of Henan University, Kaifeng475001, Henan , China; 2. Pharmaceutical Collge of Henan University, Kaifeng47 5001, Henan , China |
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| Abstract: | Objective: To synthesize(DA-6) plant growth hormone with modifying titanium sulfate as catalyst in the synthesis of(DA-6) plant growth hormone.Methods: The optimized condition was obtained by orthogonal experiments.Results: The moler ratio of diethylamino alcohol to hexanoic acid was 1.1∶1,reaction time was 10h,the amount of catalyst was 0.033mol/mol hexanoic acid.The transformation of the product could be over 95%.Conclusion: The optimized condition is suitable and feasible,which provides scientific evidence for the industrial production. |
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| Keywords: | modifying titanium sulfate plant growth hormone(DA-6) esterification |
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