| 环维黄杨星D对照品的建立 |
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| 引用本文： | 徐新军,张正行,安登魁,盛龙生.环维黄杨星D对照品的建立[J].中药新药与临床药理,2004,15(2):110-112. |
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| 作者姓名： | 徐新军 张正行 安登魁 盛龙生 |
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| 作者单位： | 1. 广州市药品检验所,广州,510160
2. 中国药科大学药学院,南京,210009 |
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| 摘 要： | 目的建立环维黄杨星D对照品.方法采用热分析、HPLC/MS、末端检测HPLC、紫外衍生HPLC、荧光衍生HPLC、TLC及非水滴定共7种方法测定环维黄杨星D对照品含量.结果热分析法不能用于环维黄杨星D纯度分析,HPLC/MS、紫外衍生HPLC、荧光衍生HPLC及末端检测HPLC四法测定的环维黄杨星D纯度一致.结论多种方法互相印证,表明该文建立的对照品分析方法可行.
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| 关 键 词： | 环维黄杨星D对照品 热分析法 非水滴定法 高效液相色谱法 高效液相色谱/质谱法 衍生作用 薄层色谱法 |
| 文章编号： | 1003-9783(2004)02-0110-03 |
| 修稿时间： | 2003年12月7日 |
Establishment of the Control of Cyclovirobuxine D |
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| XU Xinjun ,ZHANG Zhengxing,AN Dengkui,SHENG Longsheng.Establishment of the Control of Cyclovirobuxine D[J].Traditional Chinese Drug Research & Clinical Pharmacology,2004,15(2):110-112. |
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| Authors: | XU Xinjun ZHANG Zhengxing AN Dengkui SHENG Longsheng |
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| Institution: | XU Xinjun 1,ZHANG Zhengxing2,AN Dengkui2,SHENG Longsheng2 |
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| Abstract: | Objective To set up the reference standard of cyclovirobuxine D.Methods Thermal analysis,HPLC/MS,HPLC with terminal wavelength,HPLC with fluorescence derivation and with ultraviolet derivation,TLC and nonaqueous titration methods were applied to determine the content of cyclovirobuxine D control.Results Thermal analysis can not be used to analyse the purity of cyclovirobuxine D ,and HPLC/MS,HPLC with terminal wavelength,HPLC with fluorescence derivation and HPLC with ultraviolet derivation can obtain the same purity.Conclusion The methods used for the assay of cyclovirobuxine D control were practical. |
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| Keywords: | Cyclovirobuxine D control Thermal analysis Non-aqueous titration HPLC HPLC/MS Derivatization TLC |
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