| 乙肝扶正胶囊质量标准研究 |
| |
| 引用本文： | 魏萍. 乙肝扶正胶囊质量标准研究[J]. 中国药房, 2007, 18(21): 1649-1651 |
| |
| 作者姓名： | 魏萍 |
| |
| 作者单位： | 河南平顶山天宏焦化公司职工医院,平顶山市,467021 |
| |
| 摘 要： | 目的:建立乙肝扶正胶囊的质量标准。方法:采用TLC法对乙肝扶正胶囊中肉桂、当归、丹参、人参药材进行定性鉴别;采用HPLC法对2,3,5,4′-四羟基二苯乙烯-2-O-β-D-葡萄糖苷进行定量分析。结果:在薄层色谱中可检出肉桂、当归、丹参、人参相应斑点;2,3,5,4′-四羟基二苯乙烯-2-O-β-D-葡萄糖苷在20.38～203.8μg·mL~(-1)浓度范围内与峰面积积分值呈良好线性关系(r=0.999 8);平均加样回收率为103.38%,RSD=0.75%(n=6)。结论:所建标准可用于乙肝扶正胶囊的质量控制。
|
| 关 键 词： | 乙肝扶正胶囊 薄层色谱法 高效液相色谱法 质量标准 |
| 文章编号： | 1001-0408（2007）21-1649-03 |
| 收稿时间： | 2007-01-04 |
| 修稿时间： | 2007-01-042007-03-06 |
Quality Standard of Yiganfuzheng Capsules |
| |
| WEI Ping. Quality Standard of Yiganfuzheng Capsules[J]. China Pharmacy, 2007, 18(21): 1649-1651 |
| |
| Authors: | WEI Ping |
| |
| Abstract: | OBJECTIVE:To establish the quality standards of Yiganfuzheng capsules.METHODS:Cortex Cinnamomi, Radix Angelicae Sinensis,Radix Et Rhizoma Salviae Miltiorrhizae,Radix Et Rhizoma Ginseng in Yiganfuzheng capsules were identified by TLC and the content of 2,3,5,4'-terahydroxystilbene-2-O-β-D-Glucoside was determined by HPLC.RESULTS: Cortex Cinnamomi,Radix Angelicae Sinensis,Radix Et Rhizoma Salviae Miltiorrhizae,and Radix Et Rhizoma Ginseng could all be identified by TLC.2,3,5,4'-terahydroxystilbene-2-O-β-D-Glucoside showed good linear relationship within the range of 20.38～203.8μg·mL~(-1)(r=0.9998),and its average recovery was 103.38%,RSD=0.75%(n=6).CONCLUSION:The established standard can be used as a quality control for Yiganfuzheng capsules. |
| |
| Keywords: | Yiganfuzheng capsules TLC HPLC Quality standard |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
