| 药典内5种淫羊藿中黄酮类成分的反相高效液相色谱分析 |
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| 引用本文： | 郭宝林,王春兰,陈建民,肖培根.药典内5种淫羊藿中黄酮类成分的反相高效液相色谱分析[J].药学学报,1996,31(4):292-295. |
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| 作者姓名： | 郭宝林 王春兰 陈建民 肖培根 |
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| 作者单位： | 中国医学科学院药用植物研究所，中国协和医科大学药用植物研究所 |
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| 摘 要： | 报道了药典规定的5种淫羊藿──淫羊藿、箭叶淫羊藿、巫山淫羊藿、柔毛淫羊藿和朝鲜淫羊藿中9种黄酮──淫羊藿甙(icariin)、宝藿甙-Ⅰ(baohuosideI)、宝藿甙-Ⅱ(baohuosideⅡ)、淫羊藿甙A(epimedosideA)、箭藿甙B(sagittatosideB)、朝藿定B(epimedinB)、朝藿定C(epimedinC)、大花淫羊藿甙C(ikarisosideC)和大花淫羊藿甙F(ikarisosideF)的反相高效液相色谱测定。色谱柱为DISK-Cphenlyl,流动相为乙腈-乙酸液(水:36%乙酸=100:4),梯度洗脱,检测波长为272nm。
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| 关 键 词： | 高效液相色谱法 淫羊藿 箭叶淫羊藿 巫山淫羊藿 柔毛淫羊藿 朝鲜淫羊藿 黄酮类 |
| 收稿时间： | 1995-05-31 |
DETERMINATION OF 9 FLAVONOIDS IN 5 SPECIES OF EPIMEDIUM RECORDED IN CHINESE PHARMACOPOEIA BY HPLC |
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| BL Guo,CL Wang,JM Chen and PG Xiao.DETERMINATION OF 9 FLAVONOIDS IN 5 SPECIES OF EPIMEDIUM RECORDED IN CHINESE PHARMACOPOEIA BY HPLC[J].Acta Pharmaceutica Sinica,1996,31(4):292-295. |
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| Authors: | BL Guo CL Wang JM Chen and PG Xiao |
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| Abstract: | An accurate RP-HPLC method for the determination of icariin,baohuoside baohuoside Ⅱ,epimedoside A,sagittatoside B,epimedin B,epimedmc,ikarisoside C and ikarisosideF in the leaves of Epimedium brevicornum Maxim.,E. sagittatum(Sieb.et Zucc.)Maxim.,E.wushanense T.S.Ying,E.pubescens Maxim. and E. koreanum Nakai has been developed. The analytieal column wasDISK-Cphenly. The mobile phase was acetonitrile-acetic acid solution. Gradient elution was employed.The detection wavelength was 272 nm. |
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| Keywords: | HPLC Epimedium brevicornum E sagittatum E wushanense E pubescens E koreanum Flavonoids |
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