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| 黄槿化学成分的研究 | |
| 引用本文： | 张小坡,张俊清,裴月湖,许旭东,谭银丰,康胜利,刘明生. 黄槿化学成分的研究[J]. 中草药, 2012, 43(3): 440-443 |
| 作者姓名： | 张小坡 张俊清 裴月湖 许旭东 谭银丰 康胜利 刘明生 |
| 作者单位： | 1. 海南医学院药学院,海南海口571101;中国医学科学院北京协和医学院药用植物研究所,北京 100193 2. 海南医学院药学院,海南海口,571101 3. 沈阳药科大学中药学院,辽宁沈阳,100016 4. 中国医学科学院北京协和医学院药用植物研究所,北京,100193 5. 海南省南药黎药研究院,海南海口,571101 |
| 基金项目： | 海南省教育厅高校科研资助项目(Hjkj 2011-34) |
| 摘 要： | 目的研究黄槿Hibiscus tiliaceus枝叶的化学成分。方法采用硅胶柱色谱、Sephadex LH-20柱色谱分离化合物,并通过理化数据测定和波谱技术分析鉴定化合物的结构。结果从黄槿枝叶70%乙醇提取物中分离得到14个化合物,分别鉴定为木栓酮(1)、β-谷甾醇(2)、香草醛(3)、syriacusin A(4)、hibiscolactone(5)、莨菪亭(6)、臭矢菜素C(7)、反式丁烯二酸(8)、山柰酚(9)、槲皮素(10)、胡萝卜苷(11)、壬二酸(12)、丁二酸(13)、芦丁(14)。结论化合物7、9、10为首次从该属植物中分离得到,化合物3～5、8、12～14为首次从该植物中分离得到。 |
| 关 键 词： | 黄槿 木槿属 臭矢菜素C 山柰酚 槲皮素 |
| 收稿时间： | 2011-10-29 |
Chemical constituents from Hibiscus tiliaceus |
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| ZHANG Xiao-po,ZHANG Jun-qing,PEI Yue-hu,XU Xu-dong,TAN Yin-feng,KANG Sheng-li and LIU Ming-sheng. Chemical constituents from Hibiscus tiliaceus[J]. Chinese Traditional and Herbal Drugs, 2012, 43(3): 440-443 | |
| Authors: | ZHANG Xiao-po ZHANG Jun-qing PEI Yue-hu XU Xu-dong TAN Yin-feng KANG Sheng-li LIU Ming-sheng |
| Affiliation: | 1.School of Pharmaceutical Science,Hainan Medical University,Haikou 571101,China 2.Hainan Provincial Institute of South and Li Medicine Development,Haikou 571101,China 3.School of Traditional Chinese Materia Medica,Shenyang Pharmaceutical University,Shenyang 110016,China 4.Institute of Medicinal Plant Development,Chinese Academy of Medical Sciences,Peking Union Medical College,Beijing 100193,China |
| Abstract: | Objective To study the chemical constituents from the twigs and leaves of Hibiscus tiliaceus(Li medicine).Methods Compounds were isolated by repeated chromatography on silica gel and alumina gel column.Their structures were elucidated by chemical and spectroscopic methods.Results Fourteen compounds were isolated and identified as friedelin(1),β-sitosterol(2),vanillin(3),syriacusin A(4),hibiscolactone(5),scopoletin(6),cleomiscosin C(7),fumaric acid(8),kaempferol(9),quercetin(10),daucosterol(11),azelaic acid(12),succinic acid(13),and rutin(14).Conclusion This is the first report on the isolation of compounds 7,9,and 10 from the plants of Hibiscus Linn.,and compounds 3—5,8,and 12—14 from this plant. |
| Keywords: | Hibiscus tiliaceus Linn. Hibiscus Linn. cleomiscosin C kaempferol quercetin |
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